Direct polyether compound fuel cell and system
A fuel cell system, ether compound technology, applied in fuel cells, fuel cell additives, battery electrodes, etc., can solve the problems of insufficient endurance, reduce the convenience of mobile use, and increase the installation space of equipment. The effect of high energy-to-electrical conversion energy efficiency, improved safety factor and short filling time
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[0050] In some more specific embodiments, the anode catalyst is selected from any one of a composite of a Pt-Ru-Bi catalyst and an acidic polymer catalyst or a composite of a platinum carbon catalyst and an acidic polymer catalyst, preferably Pt -Composite of Ru-Bi catalyst and acid polymer catalyst; Wherein, the preparation method of described anode catalyst comprises: Pt-Ru-Bi catalyst and / or platinum carbon catalyst, acid polymer are dispersed in the mixed solution of ethanol and water , and then adding a perfluorosulfonic acid polymer (Nafion) solution, followed by ultrasonic treatment to prepare the anode catalyst.
[0051] Further, the preparation method of the Pt-Ru-Bi catalyst includes: under a protective atmosphere, make the first mixed reaction system containing platinum compound, ruthenium compound, bismuth compound, polyethylene glycol and ethylene glycol at 100-160 Reaction at ℃ for 30-180 minutes to prepare a Pt-Ru-Bi catalyst, wherein the platinum compound inclu...
Embodiment 1
[0107] image 3 It is a typical embodiment of the present invention, a direct type direct type polyether compound fuel cell and system, the direct type polyether compound fuel cell includes: polyether membrane module (f), diffuser plate (e, g ), runner plates (d, h), collector plates (c, i), functional plates (j), insulating plates (b, r), and end plates (a, s).
[0108] Among them, the polyether membrane module is composed of an anode structure, a proton exchange membrane, and a cathode structure. The anode structure consists of an anode substrate and an anode catalyst. The anode substrate can be carbon fiber cloth, carbon fiber paper and other materials, and the anode catalyst can be composed of two parts: a catalytic material for breaking ether bonds and a catalytic material for electrocatalytic oxidation. It is worth noting that although the anode catalyst is introduced in two parts for the sake of narrative, the two are closely related and cooperate with each other. Fo...
Embodiment 2
[0126] Embodiment 2 anode catalyst preparation
[0127] Di(acetylacetonate) platinum (CAS No.: 15170-57-7), ruthenium acetylacetonate (CAS No.: 14284-93-6), and bismuth nitrate pentahydrate (CAS No. 10035-06-0) were mixed according to the molar ratio of 1 : Dissolve in ethylene glycol at a ratio of 1:0.2, the concentration of platinum ions and ruthenium ions is 0.015mol / L, and the concentration of bismuth ions is 0.003mol / L, recorded as liquid A, and stored under an inert atmosphere;
[0128] Dissolve polyethylene glycol (CAS No.: 25322-68-3) in ethylene glycol at a mass fraction of 1.5%, stir vigorously for 1 hour, mix evenly, store under an inert atmosphere after degassing, and record it as liquid B;
[0129] Take 10 parts of liquid B and heat it to 100°C under nitrogen, add 1 part of liquid A under rapid stirring, and maintain the reaction at 100°C for 1 hour, and finally raise the temperature to 150°C and maintain it for 10 minutes to stop the reaction, cool to room temper...
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