Non-ablative heat protection/heat insulation/bearing integrated material and preparation method thereof
A heat-proof, non-burning technology, applied in chemical instruments and methods, lighting and heating equipment, aerospace vehicle heat-proof devices, etc., can solve the problems of high cost, difficult to be reusable, long cycle, etc., to achieve temperature and resistance Good ablation performance, good interface bonding strength, good mechanical reinforcement and toughening effect
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Embodiment 1
[0038] The preparation method of the non-ablative heat-proof / heat-insulation / carrying integrated material, the steps are as follows:
[0039] (1) Preparation of variable density ceramic fiber reinforced skeleton
[0040] Make the bulk density 0.10g / cm 3 , a thickness of 5mm, a quartz fiber layer with a fiber diameter of 0.5~3μm as the middle layer 2, and a bulk density of 0.50g / cm 3 , a quartz fiber fabric with a thickness of 2 mm and a fiber diameter of 6-8 μm is used as the upper surface layer 1, and the bulk density is 0.50 g / cm 3 , a quartz fiber fabric with a thickness of 0.5 mm and a fiber diameter of 6 to 8 μm is used as the lower surface layer 4, the above three layers are laminated, and the quartz ceramic fiber thread 3 is used for stitching (stitch spacing 5 mm), and the three layers are formed into an integral prefabricated part; Forming molds are used (for conventional plate-shaped integral prefabricated parts, molds including upper and lower panels can be used, ...
Embodiment 2
[0050] The preparation method of the non-ablative heat-proof / heat-insulation / carrying integrated material, the steps are as follows:
[0051] (1) Preparation of variable density ceramic fiber reinforced skeleton
[0052] Make the bulk density 0.30g / cm 3 , a thickness of 60mm, a mullite fiber layer with a fiber diameter of 3~4μm as the middle layer 2, and a bulk density of 1.0g / cm 3 , a silicon carbide fiber fabric with a thickness of 4 mm and a fiber diameter of 8 to 12 μm is used as the upper surface layer 1, and the bulk density is 1.0 g / cm 3 , a quartz fiber fabric with a thickness of 0.5 mm and a fiber diameter of 6-8 μm is used as the lower surface layer 4, and the above three layers are laminated, and the silicon carbide ceramic fiber thread 3 is used for stitching (stitch spacing 30 mm), and the three layers are formed into an overall prefabricated part ; Clamping and fixing the overall prefabricated part with a forming mold to obtain a variable-density ceramic fiber ...
Embodiment 3
[0061] (1) Preparation of variable density ceramic fiber reinforced skeleton
[0062] Make the bulk density 0.23g / cm 3 , thickness 27.5mm, fiber diameter of 4 ~ 5μm aluminum silicate fiber layer as the middle layer 2, bulk density 0.75g / cm 3 , a high silica fiber fabric with a thickness of 2mm and a fiber diameter of 12-15μm is used as the upper surface layer 1, and the bulk density is 0.75g / cm 3 , a high silica fiber fabric with a thickness of 0.5 mm and a fiber diameter of 12 to 15 μm is used as the lower surface layer 4, and the above three layers are laminated, and the high silica ceramic fiber thread 3 is used for stitching (stitch spacing 20 mm), and the three layers are formed Integral prefabricated part; the integral prefabricated part is clamped and fixed by a forming mold to obtain a variable-density ceramic fiber reinforced skeleton. Among them, the middle layer is made of aluminum silicate fibers, and the upper and lower layers of the high-silica fiber fabric are...
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