A kind of bone glue modified asphalt and preparation method thereof
A technology of modified asphalt and bone glue, applied in building components, building insulation materials, buildings, etc., can solve the problems of poor fatigue performance of modified asphalt, heavy burden of road construction, complicated preparation process, etc., to reduce phase angle, improve Low temperature crack resistance, simple equipment requirements
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Embodiment 1
[0019] 1) Preparation of cellulose-reinforced BG-DOPA / Zn2+ material: After fully mixing 80g of BG and 160g of deionized water, add 7g of mixed alkali (4gNaOH+3gNa2CO3) into a 50°C water bath and continue stirring for 30min; then add 15g of DOPA, 1.5g NHS and 2.0g EDC were ultrasonically dispersed for 30min. After the mixed solution was evenly dispersed, put it into a 100°C water bath and continue stirring for 24h; add 4.2g ZnCl2 and 6g chitosan to the mixed solution, and continue to stir in a 100°C water bath for 60min. The BG-DOPA / Zn2+ compound is obtained; 10 g of cellulose is added to the BG-DOPA / Zn2+ compound, and the cellulose-reinforced BG-DOPA / Zn2+ material is obtained by ultrasonic dispersion.
[0020] 2) Preparation of Bone Glue Modified Asphalt Weigh 150g of international 70# road petroleum asphalt and place it in a water bath at 140°C. When it is heated to a molten state, add 10g of cellulose-reinforced BG-DOPA / Zn2+ material in batches, and manually stir until the mi...
Embodiment 2
[0022] 1) Preparation of cellulose-reinforced BG-DOPA / Zn2+ material: After fully mixing 100g BG and 220g deionized water, add 9g mixed alkali (4gKOH+5g K2CO3) into a 50°C water bath and continue stirring for 30min; then add 18gDOPA , 1.5g NHS, 2.0g EDC ultrasonically dispersed for 30min, put the mixture into a 100°C water bath after being evenly dispersed, and continue to stir for 24h; add 5.5gZnSO4 and 7.5g chitosan to the mixture, and continue to stir in a 100°C water bath for 60min , to obtain BG-DOPA / Zn2+ compound; 18g of cellulose was added to BG-DOPA / Zn2+ compound, and the cellulose-reinforced BG-DOPA / Zn2+ material was obtained by ultrasonic dispersion.
[0023] 2) Preparation of Bone Glue Modified Asphalt Weigh 150g of international 70# road petroleum asphalt and place it in a water bath at 140°C. When it is heated to a molten state, add 8.5g of cellulose-reinforced BG-DOPA / Zn2+ material in batches, and stir manually until mixed After there are no obvious bubbles in the...
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