A kind of high-density alloy magnetic core and its preparation method
A high-density, magnetic core technology, applied in the direction of magnetic core/yoke, transformer/inductor core, inductor/transformer/magnet manufacturing, etc., can solve the problem that the alloy core cannot achieve the expected performance, the density of the alloy core decreases, etc. problems, to achieve the effect of guaranteed performance, improved density and dimensional accuracy, and increased production costs
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Embodiment 1
[0034] A kind of high-density alloy magnetic core, its preparation method comprises the following steps:
[0035] 1) Mixing iron oxide powder and bismuth oxide at a mass ratio of 1:0.05 to obtain a prefabricated green body powder with a sintering temperature of 750°C and a sintering shrinkage rate of 19.5%;
[0036] 2) Mix preform powder and polyvinyl alcohol resin (number average molecular weight: 21000g / mol) according to the mass ratio of 1:0.01, granulate, dry at 100°C for 1.5h, and press under 300MPa pressure to obtain a preform with a hollow structure body (the prefabricated body is in the shape of a cuboid with cylindrical holes inside; the density of the prefabricated body is 65% of the theoretical density; the structural diagram of the prefabricated body is shown in figure 1 shown);
[0037] 3) Mix FeSiCr powder with a particle size of 6 μm to 55 μm and a Ti coating with a thickness of 15 nm on the surface and polyvinyl alcohol resin (number average molecular weight 2...
Embodiment 2
[0040] A kind of high-density alloy magnetic core, its preparation method comprises the following steps:
[0041] 1) Mix magnesium oxide powder, bismuth oxide and copper oxide in a mass ratio of 1:0.03:0.03 to obtain a prefabricated green body powder with a sintering temperature of 830°C and a sintering shrinkage rate of 21%;
[0042] 2) Mix prefabricated body powder, polyvinyl alcohol resin (number average molecular weight 21000g / mol) and acrylic resin (number average molecular weight 19000g / mol) according to the mass ratio of 1:0.03:0.03, granulate, and dry at 100°C for 1.5h. Squeeze under 300MPa pressure, obtain the prefabricated green body of hollow structure (prefabricated green body is cuboid shape, and cylindrical hole is arranged inside; The density of prefabricated green body is 50% of theoretical density; The structural representation of prefabricated green body is as follows figure 1 shown);
[0043] 3) Mix FeSi powder with a particle size of 6 μm to 55 μm and a su...
Embodiment 3
[0046] A kind of high-density alloy magnetic core, its preparation method comprises the following steps:
[0047] 1) Mix NiZn ferrite powder, bismuth oxide and calcium oxide at a mass ratio of 1:0.03:0.03 to obtain a prefabricated body powder with a sintering temperature of 800°C and a sintering shrinkage rate of 18.5%;
[0048] 2) Mix prefabricated body powder and acrylic resin (number average molecular weight 19000g / mol) according to the mass ratio of 1:0.05, granulate, dry at 90°C for 3 hours, and press under 300MPa pressure to obtain a hollow structure prefabricated body (prefabricated The green body is in the shape of a cuboid with cylindrical holes inside; the density of the prefabricated green body is 60% of the theoretical density; the structural diagram of the prefabricated green body is as follows figure 1 shown);
[0049] 3) Mix FeNi powder with a particle size of 6 μm to 55 μm and a Cr coating with a thickness of 10 nm on the surface and acrylic resin (number aver...
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