Preparation method of magnetic response green sand cavity with excellent collapsibility
A green sand, magnetic response technology, applied in casting equipment, molds, cores, etc., can solve the problems of large vibration and noise in the production area, poor collapsibility, time-consuming and labor-intensive, etc. Effect
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Embodiment 1
[0035] A method for preparing a magnetically responsive green sand cavity with excellent collapsibility, the specific preparation method is as follows:
[0036] 1) Dissolve 240g of sodium oleate in 2.5L of deionized water, then add 2L of calcium chloride aqueous solution with a mass fraction of 1.11%, and stir magnetically for 1 hour, then add 2.5L of 1.12% sodium dihydrogen phosphate dihydrate Aqueous solution, continued magnetic stirring for 400min, then transferred to a hydrothermal reaction kettle with a capacity of 10L, sealed and heated to 210°C, kept for 36h, and the hydrothermal reaction product was washed three times with ethanol and deionized water, and dried to obtain hydroxyapatite Stone nanowires;
[0037] 2) Dissolve 0.45M antimony potassium tartrate in 25.4mL deionized water, stir magnetically for 20min to make it dissolve, add 0.15gPVP-K30 and continue stirring for 15min until it dissolves, then add 0.9MTAA to the mixed solution, stir magnetically for 40min to ob...
Embodiment 2
[0042] A method for preparing a magnetically responsive green sand cavity with excellent collapsibility, the specific preparation method is as follows:
[0043] 1) Dissolve 288g of sodium oleate in 3L of deionized water, then add 2.4L of calcium chloride aqueous solution with a mass fraction of 1.11%, and after magnetic stirring for 1 hour, add 3L of an aqueous solution of sodium dihydrogen phosphate dihydrate with a mass fraction of 1.12% , continue magnetic stirring for 30 minutes, then transfer to a hydrothermal reaction kettle with a capacity of 12L, seal and heat to 200°C, keep warm for 35 hours, wash the hydrothermal reaction product with ethanol and deionized water three times respectively, and obtain hydroxyapatite after drying Nanowires;
[0044] 2) Dissolve 0.4M antimony potassium tartrate in 33.8mL deionized water, stir magnetically for 20min to make it dissolve, add 0.16gPVP-K30 and continue stirring for 15min until it dissolves, then add 0.8MTAA to the mixed solut...
Embodiment 3
[0049] A method for preparing a magnetically responsive green sand cavity with excellent collapsibility, the specific preparation method is as follows:
[0050] 1) Dissolve 288g of sodium oleate in 3L of deionized water, then add 2.4L of calcium chloride aqueous solution with a mass fraction of 1.11%, and after magnetic stirring for 1 hour, add 3L of an aqueous solution of sodium dihydrogen phosphate dihydrate with a mass fraction of 1.12% , continue magnetic stirring for 30 minutes, then transfer to a hydrothermal reaction kettle with a capacity of 12L, seal and heat to 200°C, keep warm for 35 hours, wash the hydrothermal reaction product with ethanol and deionized water three times respectively, and obtain hydroxyapatite after drying Nanowires;
[0051] 2) Dissolve 0.5M antimony potassium tartrate in 37.5mL deionized water, stir magnetically for 20min to dissolve, add 0.27gPVP-K30 and continue stirring for 15min until it dissolves, then add 1.0MTAA to the mixed solution, sti...
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