Large mode field single-mode radiation-resistant erbium-ytterbium co-doped optical fiber and preparation method thereof
A radiation-resistant, large-mode-field technology, applied in cladding optical fiber, glass manufacturing equipment, glass fiber products, etc., can solve the problems of performance degradation and failure of erbium-ytterbium co-doped optical fiber, and improve the stability of radiation-resistant reinforcement , large mode field area, and the effect of reducing the refractive index
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preparation example Construction
[0046] The preparation method of the large-mode field single-mode radiation-resistant erbium-ytterbium co-doped optical fiber comprises the following steps:
[0047] Step 1), using a quartz tube as a deposition liner, wherein the thickness of the quartz deposition tube is 0.5-1.0 mm, using MCVD combined with a chelate vapor deposition method to prepare a fiber core, after preheating and impurity removal treatment, according to the core component flow rate The flow rate of the reaction material and oxygen is designed and set, and the deposition temperature is 1600-1900 ° C. The annular outer core layer 3, the annular depressed core layer 2, and the central core layer 1 are sequentially deposited, and shrunk into a solid mandrel by a single shrinking process. Among them, the hydrogen flow rate is 90~120sccm;
[0048] Step 2), according to the requirement of the optical fiber core wrapping ratio, adopt the sleeve technology to coat the quartz tube on the core rod, form the inner ...
Embodiment
[0060] The preparation method of erbium-ytterbium co-doped optical fiber preform is the same as that of the comparative example, the deposition liner adopts 28 / 26mm quartz tube (28mm is the outer diameter of the quartz deposition tube, 26mm is the inner diameter of the quartz deposition tube), and the reaction materials are SiCl respectively 4 , Er(TMHD) 3 , Yb(TMHD) 3 , Ce(TMHD) 3 , POCl 3 , SiF 4 etc., the specific flow rate is shown in Table 2, the annular outer core layer 3, the annular depressed core layer 2, and the central core layer 1 are deposited in sequence, and the deposition temperature is 1850°C. After the deposition, the quartz tube was shrunk into a solid rod by adopting a single-shot shrinking process with a hydrogen flow rate of 90-120 sccm. The difference is that an outer layer 5 is added to the outer layer of the preform of the comparative example, and the outer layer 5 is a sunken fluorine-doped layer, which is prepared by plasma chemical vapor deposit...
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