Method for concentrating mineral solid waste low-concentration occurrence rare and precious elements and co-producing high-grade aluminum-silicon raw materials
A high-grade, elemental technology, applied in the preparation/processing of silicon oxide, rare earth metal oxides/hydroxides, rare earth metal compounds, etc., can solve the problems of high-value utilization of silicon and aluminum, extraction interference, etc. Effectiveness of resource utilization and low-carbon eco-efficiency, avoiding acid leaching process, improving process energy efficiency and economy
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0025] A method for concentrating rare and precious elements in low-concentration mineral solid waste and co-producing high-grade aluminum-silicon raw materials, comprising the following steps:
[0026] (1) At a temperature of 800°C and a pressure of 0.1 MPa, dissolve fly ash containing a total concentration of rare earths of 131 μg / g in sodium carbonate solution to activate the silicon-aluminum crystal phase in fly ash, fly ash and sodium carbonate The mass ratio is 1:1 to obtain a mixed solution containing sodium silicon aluminum salt;
[0027] (2) At normal temperature and under the condition of a pressure of 0.1MPa, add ammonium chloride to the mixed solution obtained in step (1), the mass ratio of ammonium chloride to the mixed solution is 0.01:1, and obtain a compound containing strong alkali silicon oxide, strong alkali Liquid phase products of carbonates and weak bases and strong salts, solid phase products and gas phase products of ammonia adsorbed on the surface of r...
Embodiment 2
[0031] Same as Example 1, the difference is: in step (1), the mass ratio of fly ash and sodium carbonate is 3:1, and the reaction conditions are temperature 900 ° C, pressure 0.1MPa; in step (2), ammonium chloride and The mass ratio of the mixed solution is 0.1:1, and the reaction conditions are a temperature of 25° C. and a pressure of 0.1 MPa.
[0032] The total extraction efficiency of rare earth is 78.7%, and the yield of silicon oxide is 41.9%.
Embodiment 3
[0034] Same as Example 1, except that the reaction conditions in step (2) are a temperature of 25° C. and a pressure of 8 MPa.
[0035] The total extraction efficiency of rare earth is 82.9%, and the yield of silicon oxide is 43.2%.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com