High-temperature-resistant heat-insulating protective clothing and preparation process thereof
A technology of protective clothing and high temperature resistance, which is applied in the field of protective clothing, can solve the problems of poor heat insulation of protective clothing, inability to block heat energy from the protective clothing, and unsatisfactory flame retardant effect of protective clothing, so as to inhibit thermal decomposition and improve resistance Oxidation, improve the effect of poor compatibility
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Embodiment 1
[0048] This embodiment is a high temperature-resistant and heat-insulating protective clothing, which is prepared by the following steps:
[0049] S91: Select sulfonamide fabrics, use post-finishing flame retardants for flame-retardant finishing, and obtain flame-retardant layers;
[0050] S92: Soak the aramid fiber fabric in the antistatic liquid, dip and dry it, and coat a layer of polytetrafluoroethylene coating on the surface of the fabric, and dry it to obtain an antistatic breathable layer;
[0051] S93: compound the antistatic breathable layer, heat insulation layer and flame retardant layer in sequence;
[0052] S94: According to the size specifications of the protective clothing, the compounded fabrics are cut and garment-made to obtain high-temperature-resistant and heat-insulating protective clothing;
[0053] The insulation layer is prepared by the following steps:
[0054] S11: Cut the sulfonamide fabric to the specifications required for protective clothing, pu...
Embodiment 2
[0065] The difference between this embodiment and embodiment 1 is:
[0066] The insulation layer is prepared by the following steps:
[0067] S11: Cut the sulfonamide fabric to the specifications required for protective clothing, put it into a Soxhlet extractor and wash it with anhydrous ether for 5 hours, then wash it with distilled water, and dry it at 80°C for later use;
[0068] S12: Mix 15g of tetraethyl orthosilicate and absolute ethanol as the solvent, then add it into a three-neck flask equipped with a stirrer and a condensing device, stir at 50°C for 20min, and mix 14mL of distilled water and 5g of hydrochloric acid solution under constant stirring Add the mixed liquid drops into the three-necked flask, control the dropping rate to 1 drop / s, react for 3h, pour the reaction liquid in the flask into the beaker, and finally age at 25°C for 24h to obtain Si0 2 Dispersions;
[0069] S13: mix HS-25 silica sol, Si0 2 The dispersion liquid and distilled water are prepared ...
Embodiment 3
[0078] The difference between this embodiment and embodiment 1 is:
[0079] The insulation layer is prepared by the following steps:
[0080] S11: Cut the sulfonamide fabric to the specifications required for protective clothing, put it into a Soxhlet extractor and wash it with anhydrous ether for 6 hours, then wash it with distilled water, and dry it at 85°C for later use;
[0081] S12: Mix 15g of tetraethyl orthosilicate and absolute ethanol as a solvent, then add it into a three-necked flask equipped with a stirrer and a condensing device, stir at 70°C for 40min, and mix 14mL of distilled water and 5g of hydrochloric acid solution under constant stirring Add the mixed solution droplet into a three-necked flask, control the dropping rate to 2 drops / s, react for 5h, pour the reaction solution in the flask into a beaker, and finally age at 45°C for 48h to obtain Si0 2 Dispersions;
[0082] S13: mix HS-25 silica sol, Si0 2 The dispersion liquid and distilled water are prepar...
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