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Reaction-enhanced pre-paved waterproof coiled material and preparation method thereof

A waterproofing membrane, reaction enhancement technology, applied in the direction of adhesive types, building insulation materials, roofing using flexible materials, etc. The effect of improving waterproof safety, improving technical level, and improving bonding strength

Pending Publication Date: 2022-07-29
LIAONING BENTENAI TECH DEV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Commonly used viscous reducing materials are usually sand or stones. The use of these materials can prevent the self-adhesive layer from sticking to a certain extent, but it will also reduce the adhesion between the waterproof membrane and the post-cast concrete to a certain extent. junction performance
Especially for the asphalt-based polyester tire pre-paved waterproofing membrane, sand is used as the adhesion-reducing layer material, which often makes the bonding strength between the waterproofing material and the post-cast concrete not meet the national standard requirements, which limits the application of this type of material. In addition, during the construction of pre-paved waterproof membranes, it is often encountered that post-cast concrete construction cannot be carried out immediately after laying, and the self-adhesive on the surface is exposed for a long time outside, affected by dust, sand, ultraviolet light aging, etc., and post-cast concrete Significant decrease in cohesive force, unsatisfactory anti-water channeling effect and other problems have seriously affected the application of pre-laid waterproof membranes
[0005] Therefore, a reaction-enhanced pre-applied waterproofing membrane was developed to improve the comprehensive performance of the pre-applied waterproofing membrane and expand the existing pre-applied waterproofing membrane. Its scope of application is of great significance

Method used

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  • Reaction-enhanced pre-paved waterproof coiled material and preparation method thereof
  • Reaction-enhanced pre-paved waterproof coiled material and preparation method thereof
  • Reaction-enhanced pre-paved waterproof coiled material and preparation method thereof

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preparation example Construction

[0046] The preparation method of above-mentioned a kind of reaction-enhanced type pre-laid waterproof roll material, comprises the steps:

[0047] Step 1: prepare the modified epoxy resin by reacting rosin or hydrogenated rosin with epichlorohydrin;

[0048] Step 2: blending the modified epoxy resin with polyvinyl alcohol, plasticizer, solid epoxy resin, filler and auxiliary agent to prepare a reactive reinforced bonding protective layer;

[0049] Step 3: blend the modified epoxy resin with butyl rubber, polyvinyl alcohol, filler and auxiliary agent to prepare an adhesive;

[0050] Step 4: composite the self-adhesive layer and the main material layer by dipping, scraping or hot pressing process to obtain a single-sided self-adhesive main material layer or a double-sided main material layer;

[0051] Step 5: Cover one side of the self-adhesive layer of the single-sided self-adhesive main material with an adhesive, and coat the adhesive with a reactive reinforced bonding protec...

Embodiment 1

[0071] Add epichlorohydrin to the hydrogenated rosin according to the mass ratio of 2.2:1, wherein the epichlorohydrin is slightly excessive, and stir at 95°C to fully dissolve the rosin; add 1.5% mass fraction of the rosin to the fully dissolved rosin. Tetrabutylammonium iodide, heated and stirred for 3 hours at 95°C, ended the reaction, and cooled to room temperature; then, water was added to fully wash the product, and the water-soluble catalyst tetrabutylammonium iodide was removed to obtain a water-containing intermediate product; A mixed solvent of dichloromethane / ethyl acetate / xylene with a volume ratio of 1:3:1 was added to the intermediate product of 1:3:1, and after mixing evenly, it was allowed to stand for 48 hours, and a liquid separation treatment was performed to remove excess water in the intermediate product. Under the condition of 80°C, the intermediate product containing dichloromethane / ethyl acetate / xylene was rotary evaporated, and the solvent and hydrogen ...

Embodiment 2

[0077] Add epichlorohydrin to the rosin according to the mass ratio of 2.5:1, wherein the epichlorohydrin is slightly excessive, and stir at 90°C to fully dissolve the rosin; add 1% mass fraction of tetrafluoroethylene to the fully dissolved rosin. Butylammonium bromide, heated and stirred for 5 hours at 95°C, ended the reaction, and cooled to room temperature; then, water was added to fully wash the product, and the water-soluble catalyst tetrabutylammonium bromide was removed to obtain a water-containing intermediate product; A mixed solvent of dichloromethane / xylene with a volume ratio of 1:4 was added to the intermediate product, and after mixing evenly, it was allowed to stand for 48 hours, and a liquid separation treatment was performed to remove excess water in the intermediate product. Under the condition of 70°C, the intermediate product containing dichloromethane / xylene solvent was rotary evaporated, and the solvent and hydrogen chloride were removed to obtain the ros...

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Abstract

The invention provides a reaction-enhanced pre-laid waterproof roll and a preparation method thereof. The waterproof roll is composed of a reaction-enhanced combined protective layer, a self-adhesive layer, a main material layer, and / or an adhesive, and / or an isolating layer. Wherein the reaction type reinforced combined protective film is composed of polyvinyl alcohol, solid epoxy resin, modified epoxy resin, filler and auxiliaries, and the structure of the reaction type reinforced combined protective film is a non-woven fabric with the thickness of 0.5 mm-5 mm, a film with the thickness of 0.2 mm-2 mm or a layered structure with the thickness of 0.2 mm-5 mm formed by compounding the film and the non-woven fabric. The problems of foot sticking on the surface of the coiled material, difficulty in construction, reduction of bonding strength with post-poured concrete due to the action of rainwater, dust, silt and ultraviolet aging and the like in the building waterproof construction process can be avoided, the service life of the pre-paved waterproof material is prolonged, the waterproof safety of building engineering is greatly improved, resource waste is reduced, and the construction cost is reduced. Wide application prospects are realized.

Description

technical field [0001] The invention discloses and relates to the technical field of novel building waterproof materials, in particular to a reaction-enhanced pre-laid waterproofing membrane and a preparation method thereof. Background technique [0002] Construction safety is closely related to the national economy and people's livelihood, and has always attracted much attention. The same life span of building envelope materials and main structures has always been the focus of attention in the field of building safety. As a layer of protective outerwear for buildings, the performance of waterproof materials directly affects the service life of buildings. [0003] At present, there are many kinds of waterproof materials. According to different construction methods, waterproofing membranes can be divided into asphalt waterproofing membranes, synthetic polymer waterproofing membranes, pre-laid waterproofing membranes, wet-laid waterproofing membranes and self-adhesive waterpr...

Claims

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Application Information

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IPC IPC(8): C09J7/29C09J7/30C09J123/22C09J129/04C09J163/00C08L29/04C08L63/00E02D31/02E04B1/66E04D5/10
CPCC09J7/29C09J7/30C09J123/22C08L29/04E04B1/665E04D5/10E02D31/025C09J2203/346C09J2301/122C09J2301/16C08L63/00
Inventor 齐文张艳玲戚丁文杨林袁仁勇
Owner LIAONING BENTENAI TECH DEV
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