Biological activity glass ceramics capable of cutting and its preparation method

A bioactive glass and ceramic technology, applied in the field of silicate materials, can solve the problems of difficult processing and difficult application of bioceramics, and achieve the effects of easy operation, good bioactivity and biocompatibility, and mature technology

Inactive Publication Date: 2006-04-05
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the processing of ceramic materials is difficult, and the shape of human bones and teeth varies greatly due to differences in indivi

Method used

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  • Biological activity glass ceramics capable of cutting and its preparation method
  • Biological activity glass ceramics capable of cutting and its preparation method
  • Biological activity glass ceramics capable of cutting and its preparation method

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] Embodiment 1: by SiO 2 51.6%, Al 2 o 3 10.4%, MgO13.3%, NaF14.8%, CaHPO 4 6.3%, CaCO 3 2.7%, CaF 2 Mix 1.0% ingredients; pour into an alumina crucible, melt in a silicon-molybdenum rod furnace at 1500°C for 2 hours, and the heating rate is 5°C / min; 74μm or less; these glass powders are remelted under the same conditions and then cast into graphite molds. Before that, the molds were heated to 500-600°C, and the graphite molds were immediately moved into the heating furnace and kept at 650°C for 1 hour. Cool to obtain a glass matrix; then heat the glass matrix from room temperature to 925°C for 6 hours at a heating rate of 10°C / min, and take it out after cooling to room temperature with the furnace. After processing and grinding the prepared glass ceramics, the size is 3×4×35mm. The flexural strength is 110MPa and the elastic modulus is 8GPa by using the three-point bending method on a CSS-44100 electronic universal testing machine.

[0014] Or after obtaining the g...

Embodiment 2

[0017] Embodiment 2: by SiO 2 51.6%, Al 2 o 3 10.4%, MgO13.3%, NaF14.8%, CaHPO 4 6.3%, CaCO 3 2.7%, CaF21.0% ingredients and mix well; pour into alumina crucible, melt in silicon molybdenum rod furnace at 1500°C for 2 hours, heating rate is 5°C / min; pour molten glass into water to cool, After drying, ball mill to less than 74μm; these glass powders are remelted under the same conditions and cast into graphite molds. Before that, the molds were heated to 500-600°C, and the graphite molds were immediately moved into the heating furnace and kept at 650°C. After 1 hour, cool with the furnace to obtain the glass matrix; then raise the temperature of the glass matrix from room temperature to 1050°C for 6 hours at a heating rate of 10°C / min, and take it out after cooling to room temperature with the furnace. After processing and grinding the prepared glass ceramics, the size is 3×4×35mm. The flexural strength is 129MPa and the elastic modulus is 11GPa by three-point bending metho...

Embodiment 3

[0021] Embodiment 3: by SiO 2 45.9%, Al 2 o 3 9.2%, MgO11.8%, NaF13.1%, CaHPO 4 12.6%, CaCO 3 5.4%, CaF 2 Mix 2.0% ingredients; pour into an alumina crucible, melt in a silicon-molybdenum rod furnace at 1500°C for 2 hours, and the heating rate is 5°C / min; pour the molten glass into water to quench, dry and ball mill to 74μm or less; these glass powders were remelted under the same conditions and then cast into graphite molds; before the mold was heated to 500-600°C, the graphite mold was immediately moved into the heating furnace and kept at 650°C for 1 hour and then the furnace Cool to obtain a glass matrix; then heat the glass matrix from room temperature to 925°C for 6 hours at a heating rate of 10°C / min, and take it out after cooling to room temperature with the furnace. The obtained glass-ceramic samples are processed and polished, and the size is 3×4×35mm. The flexural strength is 134MPa and the elastic modulus is 12GPa by three-point bending method on a CSS-44100 e...

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Abstract

The invention relates to silicate material field used in repair and substitution for bone and tooth. Wherein, mixing materials with weight share in alumina ball mill tank; putting into alumina crucible, hot smelting in silicomolybdic bar furnace; pouring fused glass into water for quenching, drying and smashing; remelting the glass powder to cast in graphite mould at 500-700Deg for one hour; cooling to room temperature and obtaining even glass parent body; heating to 800-110Deg for 4-24h to separate controlled glass ceramic contained fluorine bronze mica and fluorapatite. The product has bending strength and elastic modulus fit to mechanical property of bone and teeth of human body, and can generate strong chemical bond with human bone group. This invention is simple and convenient to operate.

Description

Technical field: [0001] The invention relates to the field of silicate materials, in particular to a machinable bioactive glass ceramic and a preparation method thereof. The material is applied to the repair and replacement of bone and tooth defects. Background technique: [0002] Traditional medical biomaterials are mostly titanium alloys, stainless steel, cobalt-chromium-molybdenum alloys, polymer materials PMMA, etc. Due to poor biocompatibility, these materials are easily implanted into the human body as bone and tooth substitute materials, and fibrous cysts are easily formed. It forms a tight chemical bond with bone tissue and is easy to loosen and fall off. In recent years, bioceramics, as a new type of medical biomaterial, has attracted extensive attention. However, the processing of ceramic materials is difficult, and the shape of human bones and teeth varies greatly due to differences in individuals and specific parts. Therefore, the difficulty of processing biocer...

Claims

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Application Information

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IPC IPC(8): C03C10/06C03C10/08C03B32/02
CPCC03C10/00C03C4/0007
Inventor 刘咏向其军单小宏盛小娴
Owner CENT SOUTH UNIV
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