Composite for improving interfacial effect of photoresist dry film and barrier and preparation and usage method thereof
A photoresist and composition technology, applied in the manufacture of discharge tubes/lamps, the manufacture of ships or lead wires, the manufacture of cold cathodes, etc., can solve the problem that the surface layer of the barrier cannot be bonded, the interface effect is poor, and the barrier collapse and other problems, to achieve the effect of improving interface effect, small surface tension and reducing collapse
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[0035] Example 1
[0036] 200 g of diethylene glycol methyl butyl ether acetate, 100 g of butyl methacrylate, and 10 g of ethyl cellulose were mixed and stirred until completely dissolved. Add 20g of glass powder, wherein, based on the total weight of the glass powder, the mass ratio of the glass powder composition is: 0.5wt% SiO 2 , 50wt% ZnO, 35wt% B 2 O 3 , 0.2wt% Na 2 O, 14wt% BaO, and 0.3wt% K 2 O. Then, 100 g of 2-hydroxyethyl methacrylate, 5 g of dibutyl phthalate, and 5 g of isopropanol were added and stirred for 5 hours. Continue to stir until the bubbles disappear, set aside. Then, a lead-free barrier is fabricated using a technique known to those skilled in the art. The composition prepared above is evenly brushed on the barrier wall and dried. Paste the DFR film on the barrier layer, and produce the DFR film pattern through the traditional exposure and development process. The pattern is etched by the sandblasting etching method to simultaneously etch away the com...
Example Embodiment
[0037] Example 2
[0038] 200 g of diethylene glycol methyl butyl ether acetate, 100 g of butyl methacrylate, and 10 g of ethyl cellulose were mixed and stirred until completely dissolved. Add 35g of glass powder, wherein, based on the total weight of the glass powder, the mass ratio of the glass powder composition is: 3wt% SiO 2 , 40wt% ZnO, 35wt% B 2 O 3 , 0.2wt% Na 2 O, and 21.8wt% BaO. Add 130 g of hydroxymethacrylate, 5 g of dibutyl phthalate, and 5 g of isopropanol, and stir for 5 hours. The stirring was continued until the bubbles disappeared, and the composition of Example 2 was obtained. Then, using the above-prepared composition, the barrier ribs were manufactured by the same method as in Example 1.
Example Embodiment
[0039] Example 3
[0040] 200 g of diethylene glycol methyl butyl ether acetate, 100 g of butyl methacrylate, and 10 g of ethyl cellulose were mixed and stirred until completely dissolved. Add 10g of glass powder, wherein, based on the total weight of the glass powder, the mass ratio of the glass powder composition is: 5wt% SiO 2 , 30wt% ZnO, 45wt% B 2 O 3 , 5wt% Na 2 O, 12wt% BaO, and 3wt% K 2 O. 180 g of 2-hydroxyethyl methacrylate, 5 g of dibutyl phthalate, and 5 g of isobutanol were added and stirred for 5 hours. The stirring was continued until the bubbles disappeared, and the composition of Example 3 was obtained. Then, using the above-prepared composition, the barrier ribs were manufactured by the same method as in Example 1.
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