Biomedical Mg-Sn-Mn series magnesium alloy and plate rolling process thereof
A mg-sn-mn, biomedical technology, applied in the field of alloys, can solve the problems of unclear biological effects, poor room temperature plasticity, etc., and achieve the effect of improving room temperature plasticity and strength, improving corrosion resistance, and good plasticity
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Embodiment 1
[0028] Using pure magnesium ingot (purity 99.95%), pure tin ingot (purity 99.9%) and Mg-9.7%Mn master alloy, according to Mg-3Sn-0.5Mn alloy composition (nominal composition: Sn 3%, Mn 0.5%, impurity elements Fe 6 / CO 2 Under the protection of mixed gas, it is poured into the metal mold for gravity casting. The metallographic structure of the as-cast Mg-3Sn-0.5Mn alloy obtained by the present invention is as follows: figure 1 shown.
Embodiment 2
[0030] Using pure magnesium ingot (purity 99.95%), pure tin ingot (purity 99.9%) and Mg-9.7% Mn master alloy, according to Mg-3Sn-1Mn alloy composition (nominal composition: Sn 3%, Mn 1%, impurity element Fe 6 / CO 2 Under the protection of mixed gas, it is poured into the metal mold for gravity casting. The metallographic structure of the as-cast Mg-3Sn-1Mn alloy obtained by the present invention is as follows: figure 2 shown. The above-mentioned as-cast Mg-3Sn-1Mn alloy is subjected to high-temperature short-term solution treatment (solution treatment temperature is 555 ° C, holding time is 10-40min), and its phase composition, that is, the X-ray diffraction (XRD) pattern is as follows image 3 shown.
Embodiment 3
[0032] Before rolling the Mg-3Sn-0.5Mn alloy ingot described in Example 1, adopt two kinds of homogenization heat treatment processes of traditional solution treatment and high-temperature short-time solution treatment and traditional solution treatment respectively, and the obtained rolled Mg The phase composition of -3Sn-0.5Mn alloy is the X-ray diffraction (XRD) pattern as shown in Figure 4 Rolling state 1 and rolling state 2 are shown. Rolling deformation after homogenization heat treatment: rough rolling billet opening temperature is 400-450°C, pass reduction 10-15%; intermediate rolling temperature is 350-400°C, pass reduction can reach 50-60% ; Finish rolling temperature is 260~350℃, pass reduction is 5-10%. With the above rolling process, the rolling reduction exceeds 90% without cracks. The metallographic structure of the obtained as-rolled Mg-3Sn-0.5Mn alloy is as follows Figure 5 As shown, it can be seen from the figure that the grains of the magnesium alloy af...
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