Cleaner production method of functional lignin
A clean production, lignin technology, applied in the direction of biofuel, fermentation, etc., can solve the problems of waste, can not be fully utilized and recycled, and achieve the effect of reducing material consumption, good economic benefits, and reducing acidity
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Embodiment 1
[0030] Embodiment 1: A kind of clean production method of functional lignin
[0031] The raw material is biomass residue extracted from hemicellulose, and the steps are as follows:
[0032] (1) Steam explosion pretreatment
[0033] The explosion cavity of the steam explosion machine is 5000ml, the blasting condition is 2.0Mpa; the blasting time is 60s.
[0034] (2) Blending
[0035] Take by weighing 227g of sugar slag (equivalent to dry basis 100g) obtained after steam explosion pretreatment, put into a 1500mL beaker, and adjust the concentration of alkali with sodium hydroxide to be 1.8g / 100ml, prepare six parallel samples according to this system for subsequent use, They are respectively named sample 1, sample 2, sample 3, sample 4, sample 5, and sample 6.
[0036] (3) Hydrolysis
[0037] The above prepared reaction system was stirred and extracted at 80° C. for 2.5 h.
[0038] (4) Slag liquid separation
[0039] The above-mentioned hydrolyzed samples are suction-filte...
Embodiment 2
[0048] Embodiment 2: A kind of clean production method of functional lignin
[0049]The raw material is biomass residue extracted from hemicellulose, and the steps are as follows:
[0050] (1) Steam explosion pretreatment
[0051] The explosion cavity of the steam explosion machine is 5000ml, the blasting condition is 2.0Mpa; the blasting time is 60s.
[0052] (2) Blending
[0053] Take by weighing 227g of sugar slag (equivalent to 100g on a dry basis) obtained after steam explosion pretreatment, put into a 1500mL beaker, and adjust the concentration of alkali with sodium hydroxide to be 2.0g / 100ml, prepare six parallel samples according to this system for subsequent use, They are respectively named sample 1, sample 2, sample 3, sample 4, sample 5, and sample 6.
[0054] (3) Hydrolysis
[0055] The above prepared reaction system was stirred and extracted at 80° C. for 2.5 h.
[0056] (4) Slag liquid separation
[0057] The above-mentioned hydrolyzed samples are suction-f...
Embodiment 3
[0066] Embodiment 3: A kind of clean production method of functional lignin
[0067] The raw material is biomass residue extracted from hemicellulose, and the steps are as follows:
[0068] (1) Steam explosion pretreatment
[0069] The explosion cavity of the steam explosion machine is 5000ml, the blasting condition is 2.0Mpa; the blasting time is 60s.
[0070] (2) Blending
[0071] Take by weighing 227g of sugar slag (equivalent to dry basis 100g) obtained after steam explosion pretreatment, put into a 1500mL beaker, and adjust the concentration of alkali with sodium hydroxide to be 1.9g / 100ml, prepare six parallel samples according to this system for subsequent use, They are respectively named sample 1, sample 2, sample 3, sample 4, sample 5, and sample 6.
[0072] (3) Hydrolysis
[0073] The above prepared reaction system was stirred and extracted at 80° C. for 2.5 h.
[0074] (4) Slag liquid separation
[0075] The above-mentioned hydrolyzed samples are suction-filte...
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