Animal codonopsis pilosula polysaccharide oral solution and preparation method thereof
A technology of Codonopsis polysaccharides and oral liquid, which is applied in the field of modern Chinese veterinary drug compound preparations, can solve problems such as increased production costs, inability to efficiently extract polysaccharide components, and product efficacy discounts
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Embodiment 1
[0024] A Codonopsis polysaccharide oral liquid is composed of the following raw material ratios: Codonopsis 2000g and sodium benzoate 3g.
[0025] The above-mentioned Codonopsis polysaccharide oral liquid is prepared by the following steps:
[0026] 1. Pretreatment: Accurately weigh 2000g of Codonopsis pilosula, cut and pulverize;
[0027] 2. Petroleum ether degreasing: extract the processed Codonopsis pilosula at 80°C with 6 times the weight of the medicinal material in petroleum ether for 1 hour, filter, and take the filter residue;
[0028] 3. Ethanol reflux decolorization and impurity removal: extract the filter residue with ethanol 10 times the weight of the filter residue for 1 hour, and obtain the medicinal residue after filtration;
[0029] 4. Water extraction: Add 8 times the weight of the dregs to decoct in water for 2 times, the first time for 2 hours, the second time for 1.5 hours, combine the decoction, and filter;
[0030] 5. Removal of starch: add 24g of amyla...
Embodiment 2
[0037] A Codonopsis polysaccharide oral liquid is composed of the following raw material ratios: Codonopsis 2200g and sodium benzoate 3g.
[0038] The above-mentioned Codonopsis polysaccharide oral liquid is prepared by the following steps:
[0039] 1. Pretreatment: Accurately weigh 2200g of Codonopsis pilosula, cut and pulverize;
[0040] 2. Petroleum ether degreasing: extract the processed Codonopsis pilosula at 85°C with 8 times the weight of the medicinal material in petroleum ether for 1.5 hours, filter, and take the filter residue;
[0041] 3. Ethanol reflux decolorization and impurity removal: extract the filter residue with ethanol 10 times the weight of the filter residue for 2 hours, and obtain the medicinal residue after filtration;
[0042] 4. Water extraction: add 8 times the weight of the dregs to the decoction twice, the first time for 3 hours, the second time for 1.5 hours, combine the decoction, and filter;
Embodiment 3
[0050] A Codonopsis polysaccharide oral liquid is composed of the following raw material ratios: Codonopsis 1800g and sodium benzoate 3g.
[0051] The above-mentioned Codonopsis polysaccharide oral liquid is prepared by the following steps:
[0052] 1. Pretreatment: Accurately weigh 1800g of Codonopsis pilosula, cut and pulverize;
[0053] 2. Water extraction: Add 10 times the weight of medicinal materials and decoct twice, the first time for 3 hours, the second time for 2 hours, combine the decoction, and filter;
[0054] 3. Removal of starch: add 20g of amylase in a water bath for enzymolysis for 1 hour, after the reaction, boil water to inactivate the enzyme for 5 minutes, cool to room temperature, centrifuge at 3000r / min for 5 minutes, and take the supernatant;
[0055] 4. Concentration: the supernatant is concentrated to 2 / 3 (V / W) of the crude drug amount;
[0056] 5. Alcohol precipitation: Add 95% ethanol to the concentrated solution to make the alcohol content reach 8...
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