Hardened optical thin film and preparation method thereof

A technology of optical thin film and hard coating, which is applied in the field of preparation of optical thin film, can solve the problems of decreased adhesion, poor adhesion of inorganic deposition layer, scratched appearance, etc.

Inactive Publication Date: 2012-07-11
PANYU NANSHA YAN TIN CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, at present, most plastic film surfaces are easily scratched or scratched by mutual contact and friction. Therefore, coating or electroplating a layer of hard coating on the surface of plastic films is favored by the market. The optical poly film with surface hardening treatment Can be widely used as a protective panel for touch screens or as a substrate material for flexible ITO films
[0003] At present, there are mainly two methods for hardening the surface of polyester film. One mainly uses surface electroplating to deposit a layer of inorganic oxide film, such as silicon dioxide and antimony trioxide. The equipment investment is large, the adhesion of the inorganic deposition layer is poor and the flexibility is poor and easy to crack; the other is mainly to coat the surface with a layer of o

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Put 15 parts of UV curable resin, 30 parts of UV curable reactive dilution resin, 5 parts of Irgacure184, 0.5 parts of leveling agent, 25 parts of ethyl acetate, 15 parts of butyl acetate and 10 parts of propylene glycol monomethyl ether in the stirring tank Thoroughly stir and mix uniformly to obtain a hardened coating liquid for hardening treatment.

[0028] The coating liquid is evenly coated on the surface of the polyester film substrate by the dimple coating method, and the solvent is volatilized by infrared heating to form a hardened hard coating. After 1000mj / cm 2 It is cured by energy ultraviolet radiation to obtain a hardened polyester film. Measure its performance (see Table 1 for details)

Embodiment 2

[0030] Put 20 parts of UV curable resin, 25 parts of UV curable reactive dilution resin, 5 parts of Irgacure184, 0.5 parts of leveling agent, 25 parts of ethyl acetate, 15 parts of butyl acetate and 10 parts of propylene glycol monomethyl ether in the stirring tank Thoroughly stir and mix uniformly to obtain a hardened coating liquid for hardening treatment.

[0031] Using method is the same as embodiment 1, and the results are shown in Table 1

Embodiment 3

[0033] Put 30 parts of UV curable resin, 15 parts of UV curable reactive dilution resin, 5 parts of Irgacure184, 0.5 parts of leveling agent, 25 parts of ethyl acetate, 15 parts of butyl acetate and 10 parts of propylene glycol monomethyl ether in a stirred tank Thoroughly stir and mix uniformly to obtain a hardened coating liquid for hardening treatment.

[0034] Using method is the same as embodiment 1, and the results are shown in Table 1

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PUM

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Abstract

The invention discloses a hardened optical thin film. A hardened coating with good optical property is uniformly coated on a transparent thin film base material. The hardened coating consists of 10-90 parts of ultraviolet curable resin, 10-30 parts of ultraviolet solid activity diluted resin, 2-15 parts of light initiator, 0-3 parts of flatting agent, and 10-90 parts of solvent. The hardened optical thin film disclosed by the invention has the advantages as follows: 1, the polyester has higher heat resistance, higher melting point and controllable degradation speed; 2, titanium dioxide sediments cannot be formed in a production process since the use amount of catalyst is small, so that the maintenance and replacement period of production equipment can be prolonged; 3, the vertical and transverse tearing intensities of the polyester material are higher; and 4, the structure of the polyester is easy to control, gel is difficult to form in a reaction process, and the processed film material has no crystal points which are formed by the gel.

Description

technical field [0001] The invention relates to a method for preparing an optical film, in particular to a method for preparing an optical film with relatively high hardness. Background technique [0002] In recent years, with the rapid development of the liquid crystal display industry, products such as smartphones and touch screens are widely used in daily life, so the demand for light and thin optically transparent plastic films is also increasing day by day. However, at present, most plastic film surfaces are easily scratched or scratched by mutual contact and friction. Therefore, coating or electroplating a layer of hard coating on the surface of plastic films is favored by the market. The optical poly film with surface hardening treatment It can be widely used as a protective panel for touch screens or as a substrate material for flexible ITO films. [0003] At present, there are mainly two methods for hardening the surface of polyester film. One mainly uses surface ...

Claims

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Application Information

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IPC IPC(8): G02B1/10C08J7/04G02B1/14
Inventor 钟强锋李兆辉藤川昇陈伟梅
Owner PANYU NANSHA YAN TIN CHEM
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