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Vacuum coating preparation method of aviation organic glass and preparation thereof

A technology of vacuum coating and plexiglass, which is applied in vacuum evaporation coating, sputtering coating, ion implantation coating and other directions, can solve the problem of the adhesion between the anti-reflection coating and the spectacle lens substrate needs to be further improved, and achieve high adhesion , High light transmittance, and the effect of improving work efficiency

Inactive Publication Date: 2012-09-19
宫杰 +2
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  • Application Information

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Problems solved by technology

However, the adhesion between the AR coating and the spectacle lens substrate needs to be further improved

Method used

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  • Vacuum coating preparation method of aviation organic glass and preparation thereof
  • Vacuum coating preparation method of aviation organic glass and preparation thereof
  • Vacuum coating preparation method of aviation organic glass and preparation thereof

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Experimental program
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Embodiment Construction

[0020] 1. Transparent aviation plexiglass window plate base material (polymethyl methacrylate) coating workpiece (7), its specification is: diameter 211mm x thickness 5mm.

[0021] 2. A vertical vacuum coating device is used to continuously complete the preparation of three layers of film on the substrate and workpiece. The structure of the vacuum coating device is as follows: the vertical single-door vacuum chamber box (11) is connected with the vacuum pump group (5), the electron gun electron beam evaporation system (14) is installed on the bottom plate of the box body, and the film material with indexing is used. The four-hole crucible (17), the metal oxide film material (16) is placed in the crucible hole, the indexable baffle (12) is located 200 mm above the crucible, an ion bombardment holder (6) is located in the middle of the vacuum chamber, and the vacuum chamber top plate A vertical shaft system (8) is installed on the lower surface to drive a turntable, on which a...

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Abstract

The invention relates to a vacuum coating preparation method of an aviation organic glass (polymethylmethacrylate). A set of electronic beam evaporation and ion assisted vacuum coating device is used for continuously preparing a structure of three layers of (auxiliary-main-auxiliary) deposition film series, wherein two auxiliary film layers are respectively located on the bottom layer and the upper layer of a main film layer. The two auxiliary film layers are obtained by heating polytetrafluoroethylene resin liquid, evaporating and vaporizing, spraying into a vacuum chamber, ionizing under ion bombardment, and respectively depositing on the surface of the substrate and above the main film layer. The main film layer is deposited on a bottom layer film by film material (one of zirconium dioxide or hafnium oxide) under electronic beam evaporation and ion assisted bombardment so as to form an optical antireflection film. According to the invention, the structure of three layers of films, which is continuously prepared in vacuum, has the characteristics of high adhesion, high light transmissivity, low haze, friction resistance, weak acid and weak base corrosion resistance and the like. The preparation method provided by the invention is further suitable for vacuum coating of polycarbonate (PC) resin, and can be widely applied in industries of aviation, automobiles, car light outer covers and the like.

Description

technical field [0001] The invention relates to a preparation method of synthetic resin vacuum coating film, in particular to a preparation method of aviation plexiglass (polymethyl methacrylate) vacuum coating film. Background technique [0002] The vacuum coating of aviation plexiglass (polymethyl methacrylate) and acrylic resin (PC) materials is more and more used in the observation windows of aircraft cabins, auto parts and lamp covers. The advantages of this type of material are light weight, good transparency, and no cracking by impact, but the disadvantage is that the surface hardness is low, easy to scratch and not resistant to abrasion. Vacuum coating on the surface is an effective treatment method to improve its performance. However, the traditional vacuum coating process often leads to low adhesion strength between the surface of aviation plexiglass and the vacuum coating film, and the film layer is easy to peel off. This problem has been puzzling people, limiti...

Claims

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Application Information

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IPC IPC(8): C23C14/32C23C14/54C23C14/08C23C14/12
Inventor 宫杰刘家兴许镜明蔡中林邬纪泽
Owner 宫杰
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