Industrial preparation method of high-yield cinnamaldehyde
A cinnamaldehyde, high-yield technology, applied in the field of cinnamaldehyde preparation, can solve problems such as poor economic benefits, insufficient yield, equipment corrosion, etc., achieve the effects of reducing thermal damage, improving product yield and purity, and avoiding pollution
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0029] First configure the aqueous solution: take 2.25kg of PEG-400 and add it to 1 ton of deionized water, stir evenly, and set aside.
[0030] A. Before feeding, nitrogen purging is used to remove the oxygen in the reaction vessel, and then 50kg of strong basic anion exchange resin and the prepared aqueous solution of PEG-400 are added through the feeding kettle. The strong basic anion exchange resin used is Nanjing D201 macroporous strongly basic styrene-based anion exchange resin produced by the resin factory, then add 450kg of benzaldehyde and stir for half an hour;
[0031] B. Control the temperature at 15-20°C, add dropwise 450kg of 30% mass percent acetaldehyde aqueous solution while stirring, and add dropwise for 1 hour. After the dropwise addition, control the temperature at 25°C, and react for 3.5 hours;
[0032] C. After the reaction is completed, the reaction liquid is washed with water, and then multi-stage static stratification is carried out: put the material i...
Embodiment 2
[0035] First prepare the aqueous solution: take 2 kg of PEG-400 and add it to 1 ton of deionized water, stir evenly, and set aside.
[0036] A. Before feeding, nitrogen purging is used to remove the oxygen in the reaction vessel, and then 50kg of strong basic anion exchange resin and the prepared PEG-400 aqueous solution are added through the feeding kettle. The strong basic anion exchange resin used is Rohm &Hass Co. (Rohm and Haas company) produces Amberjet 4400 OH, then add benzaldehyde 400kg, stir for half an hour;
[0037] B. Control the temperature at 15-20°C, add dropwise 400kg of acetaldehyde aqueous solution with a mass percentage of 40% while stirring, and add the time for 1.5 hours. After the dropwise addition, control the temperature at 28°C and react for 4 hours;
[0038] C. After the reaction is completed, the reaction liquid is washed with water, and then multi-stage static stratification is carried out: put the material into the static equipment and let it stan...
Embodiment 3
[0041] First configure the aqueous solution: take 2.3kg of PEG-400 and add it to 1 ton of deionized water, stir evenly, and set aside.
[0042] A. Before feeding, use nitrogen purge to remove the oxygen in the reaction vessel, and then add 50kg of strong basic anion exchange resin and the configured PEG-400 aqueous solution through the feeding kettle. The strong basic anion exchange resin used is Mitsubishi Diaion PA produced by Chemical Industries Co.Ltd. (Mitsubishi Chemical Corporation), then add 460kg of benzaldehyde and stir for half an hour;
[0043] B. Control the temperature at 15-20°C, add 250kg of acetaldehyde aqueous solution with a mass percentage of 50% dropwise while stirring, and add dropwise for 2 hours. After the dropwise addition, control the temperature at 30°C and react for 5 hours.
[0044] C. After the reaction is completed, the reaction liquid is washed with water, and then multi-stage static stratification is carried out: put the material into the stati...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com