Chemical nickel plating solution and aluminum silicon carbide plating method
An electroless nickel plating solution and carbon silicon technology, applied in the field of metal electroplating, can solve the problems of increased surface roughness and porosity, poor bonding force of the coating on silicon carbide, material failure, etc., and achieve good coverage, stable process, The effect of easy operation
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Embodiment 1
[0016] A kind of electroplating pretreatment and primer coating process of carbon silicon aluminum material workpiece, the specific process flow is as follows:
[0017] 1. Shot peening: first, the surface of the workpiece is shot peened, using 300-mesh glass beads at a pressure of 2.5 atmospheres;
[0018] 2. Degreasing: After shot blasting, the workpiece is degreased. The components of the degreasing liquid are: 30 g / L sodium phosphate, 30 g / L sodium carbonate, 2 ml / L OP-10, The degreasing temperature is controlled at 65-70°C, and the time is about 45 seconds, and it enters the activation process after being washed with tap water;
[0019] 3. Activation: The purpose of activation is to moderately etch and roughen the silicon carbide in the carbon silicon aluminum material, so as to improve the bonding force of the coating. The composition of the activation solution is: 900ml / L nitric acid, 80g / L ammonium bifluoride, activated at 25°C for 60 seconds, and washed with two pure ...
Embodiment 2~3
[0025] Compared with Example 1, Examples 2-3 differ in the composition of the electroless nickel plating solution and the zinc dipping solution. Table 1 and Table 2 are the composition comparisons of the electroless nickel plating solution and the zinc dipping solution in Examples 2 to 3 and Example 1.
[0026] Nickel sulfate hexahydrate, g / L Sodium hypophosphite, g / L Disodium hydrogen phosphate, g / L Sodium aminotrimethylene phosphonate, g / L KIO3, mg / L Polyethylene glycol.g / L temperature, ℃ time, min Example 1 30 30 30 35 10 2.5 80 30 Example 2 25 30 25 40 8 2.5 90 20 Example 3 40 40 40 50 20 3 85 20
[0027] Sodium gluconate, g / L Sodium potassium tartrate, g / L Zinc sulfate, g / L Sodium carbonate, g / L Lithium fluoride, g / L temperature, ℃ time, s Example 1 120 60 30 5 3 20 30 Example 2 100 50 25 4 3 20 60 Example 3 120 80 40 7 5 20 30
[0028] The...
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