Anti-reflective film and production method thereof
An anti-reflection film and one-sided technology, applied in optics, instruments, optical components, etc., can solve the problems of coating hardness, scratch resistance and other performance degradation, complex preparation process of hollow particles, poor mechanical properties of hollow particles, etc., to achieve guaranteed The effect of apparent quality, high porosity and uniform pores
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Embodiment 1
[0053] Hexafluorobutyl acrylate (refractive index 1.39) 10 g,
[0054] 5nm silica 9.1 g,
[0055] 40nm silica 0.91 g,
[0056] PETA (Pentaerythritol Acrylate) 3 g,
[0057] Methacryloxypropyltrimethoxysilane 5 g,
[0058] Initiator 184 (1-hydroxy-cyclohexyl-phenyl ketone) 0.3 g,
[0059] X-22-164E (Shin-Etsu) 0.1 g,
[0060] Butanone 4 g,
[0061] 1-methoxy-2-2-propanol 36 g,
[0062] 10g of hexafluorobutyl acrylate with a refractive index of 1.39 was added to a mixed solvent composed of 36g of 1-methoxy-2-2 propanol and 4g of butanone, and after stirring and dissolving, 9.1g of 5nm silicon dioxide, 0.91 g of 40 nanometer silica, 3.0 g of PETA, 5.0 g of methacryloxypropyltrimethoxysilane, 0.3 g of initiator 184, and 0.1 g of X-22-164E were stirred and dispersed to obtain an antireflection coating solution.
[0063] The above anti-reflection coating solution was uniformly coated on a polyethylene terephthalate (PET) film base with a thickness of 80 microns, then dried at...
Embodiment 2
[0065] Hexafluorobutyl methacrylate (refractive index 1.36) 20g,
[0066] 10nm silica 25g,
[0067] 75nm silica 5g,
[0068] PETA (Pentaerythritol Acrylate) 3g,
[0069] DPHA (Dipentaerythritol Hexaacrylate) 1g,
[0070] Acryloxypropyltriethoxysilane 6g,
[0071] Initiator 184 (1-hydroxy-cyclohexyl-phenyl ketone) 0.5g,
[0072] X-22-164E (Shin-Etsu) 0.5g,
[0073] Butanone 15g,
[0074] Methyl isobutyl ketone 35g,
[0075] Add 20g of hexafluorobutyl methacrylate with a refractive index of 1.36 into a mixed solvent consisting of 35g of methyl isobutanol and 15g of butanone, stir and dissolve, then add 25g of 10nm silicon dioxide and 75nm 5g of silicon, 3g of PETA, 1g of DPHA, 6g of acryloxypropyltriethoxysilane, 0.5g of initiator 184, and 0.5g of X-22-164E were stirred and dispersed to obtain an antireflection coating liquid.
[0076] The above anti-reflection coating solution was uniformly coated on a triacetate cellulose (TAC) film base with a thickness of 80 microns,...
Embodiment 3
[0078] LINC-2A (manufactured by Kyoeisha, Japan, refractive index 1.40) 30g,
[0079] 8nm silica 15g,
[0080] 50nm silica 5g,
[0081]DPHA (Dipentaerythritol Hexaacrylate) 5g,
[0082] Methacryloxypropyldimethoxymethylsilane 7g,
[0083] Initiator 184 (1-hydroxy-cyclohexyl-phenyl ketone) 1.5g,
[0084] TPO (2,4,6,-trimethylbenzoyl-diphenylphosphine oxide) 1g,
[0085] X-22-164E (Shin-Etsu) 0.5g,
[0086] Butanone 32g,
[0087] Cyclohexanone 48g,
[0088] Add 30g LINC-2A with a refractive index of 1.4 into a mixed solvent composed of 48g cyclohexanone and 32g butanone, stir and dissolve, then add 15g of 8nm silicon dioxide, 5g of 50nm silicon dioxide, 5g of DPHA, 7 g of methacryloxypropyl dimethoxymethylsilane, 1.5 g of initiator 184, and 0.5 g of X-22-164E were stirred and dispersed to obtain an antireflection coating liquid.
[0089] Coat the above anti-reflection coating solution evenly on a triacetylcellulose (TAC) film base with a thickness of 80 microns, then dry...
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