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A kind of manufacturing method of nickel oxide-loaded ferromagnetic core

A production method and technology of nickel oxide, applied in the direction of inductance/transformer/magnet manufacturing, inorganic material magnetism, electrical components, etc., to achieve the effect of uniform grain, less cracking, and stable electromagnetic performance

Active Publication Date: 2016-05-04
TIANCHANG CITY ZHAOTIAN MAGNETOELECTRICITY TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Now the electronic communication industry needs ferrite cores with low core loss and high magnetic permeability to meet the miniaturization and high efficiency requirements of current electrical equipment, and the existing magnetic cores are difficult to meet the above requirements

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] Embodiment 1: the manufacture method of the ferromagnetic core of loading nickel oxide, comprises the following steps:

[0015] (1) Pre-fired mixture: the molar amount of mixture A is Fe 2 o 3 60mol, 32mol of manganese oxide, 0.58mol of nickel oxide, 0.14mol of ferrophosphorus powder, 0.22mol of ferrosilicon, 0.58mol of nano-zinc powder, 0.60mol of reduced iron powder and 0.25mol of dilanthanum trioxide; The following ratio components of the total weight: 300ppm Zr, 78ppm yttrium, 165ppm Al 2 o 3 , 140ppm copper powder, 360ppm chromium powder, 470ppm manganese sulfide, 720ppm molybdenum powder and 740ppm modified nano-carbon; Accurately weigh mixture A and mixture B respectively, use mixing tank to mix separately, and the stirring and mixing time under 6200 rev / min is After 2.5 hours, they are sent to the rotary kiln for pre-burning respectively, the temperature is controlled at 380°C, and the pre-burning time is 1.0-1.5 hours to obtain pre-fired mixture A and mixtur...

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PUM

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Abstract

The invention discloses a method for manufacturing a ferromagnetic core loaded with nickel oxide. The method includes steps of performing pre-sintering on a mixture A comprising Fe<3>O<4>, manganese oxide, the nickel oxide, ferro-phosphorus powder, ferrosilicon, nano-zinc powder, reduced iron powder and lanthanum trioxide and a mixture B comprising Zr, yttrium, Al<2>O<3>, copper powder, chromium powder, manganese sulfide, molybdenum powder and modified nano-carbon; then sequentially performing grinding, mixing and pulping, powder spray-drying, green body pressing and sintering processes on the mixture A and the mixture B to obtain the ferromagnetic core. The total weight of the mixture B is equivalent to that of the mixture A. The method has the advantages that owing to an optimized formulation design and the sintering process, the initial permeability of a product manufactured by the method is 14500, cracking of the sintered product is little, the qualified rate of the product reaches 92.8% at least, the product is high in grain boundary resistivity and low in porosity, crystal grains of the product are large and uniform, the impendence characteristic of the product in a high-frequency range is excellent, various electromagnetic properties of the product are stable, and the ferromagnetic core product is applicable to various electronic fields.

Description

technical field [0001] The invention relates to the field of manufacturing oxide magnetic materials, in particular to a method for manufacturing a ferromagnetic core loaded with nickel oxide. Background technique [0002] With the development of communication technology and digitalization of electronic products, new requirements are put forward for soft ferrite and components. High-performance and high-permeability magnetic cores are widely used in various basic materials for telecommunications and information, such as common-mode filters, Saturated inductors, current transformers, leakage protectors, insulation transformers, signal and pulse transformers and other fields have been widely used. Now the electronic communication industry needs ferrite cores with low core loss and high magnetic permeability to meet the miniaturization and high efficiency requirements of current electrical equipment. The existing magnetic cores are difficult to meet the above requirements. Con...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01F41/02H01F1/33C04B35/64
Inventor 徐杰杨从会黄国祥刘京州曾性儒张忠仁王玉志
Owner TIANCHANG CITY ZHAOTIAN MAGNETOELECTRICITY TECH