65results about How to "Large and uniform crystal grains" patented technology

The invention discloses a method for producing a soft magnetic core of load palladium oxide. The method comprises the following steps of: pre-burning mixtures, wherein the components of the mixture A comprise Fe3O4, manganese oxide, palladium oxide, molybdenum powder, ferrosilicon, nanoscale titanium dioxide, carbonyl iron powder and chromium powder; and the components of the mixture B comprise Nb2O5, Bi2O3, tungsten trioxide, Pd, V, manganese sulfide, molybdenum disulfide powder, and graphite powder according to the ratio equivalent to the total weight of the mixture A; then grinding, mixed pulping, spray drying of powder, pressing and sintering green bodies orderly, so as to obtain the soft magnetic core. The initial magnetic conductivity of the produced product is 13300 by optimizing the formula design and sintering technology; cracks of the sintered product are reduced; the qualified rate can be up to over 9.05%; the produced product has the characteristics of high grain boundary resistivity, low porosity, large and even grain size, excellent impedance characteristic in a high-frequency range, and stable electromagnetic property; a magnetic core product is suitable for each electronic field.

The invention discloses a nickel-oxide-based ferrite core material used for a transformer. The nickel-oxide-based ferrite core material comprises main materials and additives. The main materials comprise, by molar ratio, 60.2 mol to 66 mol of Fe2O3, 13.0 mol to 18 mol of manganese oxide, 11.3 mol to 16 mol of zinc oxide, 3 mol to 4 mol of magnesium oxide, 0.1 mol to 0.2 mol of sodium metasilicate, 0.6 mol to 1 mol of cobaltosic oxide and 0.01 mol to 0.02 mol of rare-earth composite magnetic powder. The additives comprise, by weight ratio of components to the ferrite core material, 70 ppm to 100 ppm of lithium nitride and 60 ppm to 80 ppm of ferrous sulfate. The rare-earth composite magnetic powder added into the nickel-oxide-based ferrite core material is high in magnetic energy product, stable in magnetism and simple in preparing method, and the finished product has the advantages of being high in crystal boundary resistivity, low in gas hole ratio and large and even in crystal particle.

The invention discloses a lanthanum base ferrite magnetic core material for a transformer. The lanthanum base ferrite magnetic core material comprises a main material and additives, wherein the main material comprises the following ingredients according to the mol ratio: 60.2 to 66mol of Fe2O3, 13.4 to 17mol of manganese oxide, 9.1 to 11mol of zinc oxide, 1 to 2.7mol of graphite, 0.5 to 0.8mol of tin oxide, 0.1 to 0.2mol of barium sulfate and 0.01 to 0.02mol of rare earth composite magnetism conduction powder bodies, and the additives comprise the following materials through being metered by the weight ratio of the materials to the ferrite magnetic core material: 70 to 100ppm of potassium permanganate and 60 to 70ppm of cobalt oxide. The lanthanum base ferrite magnetic core material has the advantages that the magnetic energy product of the rare earth composite magnetism conduction powder bodies added into the ferrite magnetic core material is high, the magnetism is stable, a preparing method is simple, and a finished product has the characteristics of high crystal boundary resistivity, low porosity and large and uniform crystal particles.

The invention discloses a rear-earth ferrite magnetic core material used for a transformer. The rear-earth ferrite magnetic core material comprises main ingredients and additives, wherein the main ingredients comprise the following components in molar ratio: 61.4-70 mol of Fe2O3, 16.7-20 mol of manganese oxide, 10-14.2 mol of zinc oxide, 1-2 mol of copper oxide, 0.4-0.6 mol of calcium sulfate and 0.01-0.02 mol of rear-earth composite magnetic powder; the additives comprise the following components in proportion by weight (based on the ferrite magnetic core material): 40-50 ppm of chromic oxide and 800-1000 ppm of zinc borate. The rear-earth composite magnetic powder added in the ferrite magnetic core material disclosed by the invention is high in magnetic energy product, stable in magnetism and simple in preparation method; a finished product has characteristics of high crystal boundary resistivity, low porosity, great and uniform crystalline grain.

The invention discloses a niobium-based ferrite core material used for a transformer. The niobium-based ferrite core material comprises main materials and additives. The main materials comprise, by molar ratio, 62 mol to 72.3 mol of Fe2O3, 20.1 mol to 25 mol of manganese oxide, 10 mol to 13.5 mol of zinc oxide, 0.6 mol to 0.8 mol of titanium dioxide, 0.1 mol to 0.3 mol of barium oxide and 0.01 mol to 0.02 mol of rare-earth composite magnetic powder. The additives comprise, by weight ratio of components to the ferrite core material, 60 ppm to 100 ppm of sodium silicate, 20 ppm to 60 ppm of cobaltosic oxide and 70 ppm to 100 ppm of magnesium oxide. The rare-earth composite magnetic powder added into the niobium-based ferrite core material is high in magnetic energy product, stable in magnetism and simple in preparing method, and the finished product has the advantages of being high in crystal boundary resistivity, low in gas hole ratio and large and even in crystal particle.

The present invention discloses a maifanite base ferrite magnetic core material for transformers. The maifanite base ferrite magnetic core material comprises main materials and additives, wherein the main materials comprise, by molar, 59-66.2 mol of Fe2O3, 15.7-21 mol of manganese oxide, 10.2-15 mol of zinc oxide, 1.3-2 mol of ferrocene, 1-1.2 mol of boron oxide, 0.1-0.2 mol of cobalt powder, and 0.01-0.02 mol of a rare earth composite magnetic conduction powder body, and the additives comprise, by weight (calculated as the weight of the ferrite magnetic core material), 70-100 ppm of beryllium oxide, 70-100 ppm of aluminum oxide, and 60-100 ppm of nickel. According to the ferrite magnetic core material of the present invention, the added rare earth magnetic conduction powder body has the high magnetic energy product, the magnetism is stable, the preparation method is simple, and the finished product has characteristics of high grain boundary resistivity, low porosity, and large and uniform grain.

The invention discloses a tantalum-based ferrite magnetic core material used for transformer, which comprises a main material and an additive, the main material comprises the following components according to mol ratio: 57.1-64mol of Fe2O3, 16.2-20mol of manganese oxide, 10.1-15mol of zinc oxide, 4-5.2mol of copper oxide, 0.2-1 mol of zinc borate, 1-1.3mol of barium oxide and 0.01-0.02mol of rare earth composite magnetic conductive powder; and the additive comprises the following components according to weight ratio of the additive in the ferrite magnetic core material: 30-50ppm of aluminium triphosphate, 10-20ppm of titanium tetrachloride and 40-50ppm of silicon powder. The magnetic energy product of the rare earth composite magnetic conductive powder in the ferrite magnetic core material is high, and magnetic performance is stable, preparation method is simple, and the finished product has the characteristics of high crystal boundary resistivity, low porosity and large crystal grain.

The invention discloses a preparation method of a MnZn (Manganese-Zinc) soft magnetic ferrite material containing modified tree ash. The preparation method comprises the following steps of: preparing main materials, preparing auxiliary materials, pre-burning, mixing and secondarily ball-milling the main materials and the auxiliary materials, shaping and sintering to obtain a MnZn soft magnetic ferrite magnetic core of modified tree ash. Through the addition of the modified tree ash, the MnZn soft magnetic ferrite material can play a bridge combination role among different raw materials; the used raw materials have the advantages of better distribution, high density, high grain boundary resistivity, low porosity and great and even grains; the prescription of the raw materials is reasonably improved, so that the magnetic core has higher magnetic conductivity after firing; and the indexes such as power loss, frequency feature, curie temperature, saturation flux density and the like are greatly improved.

The invention discloses a method for manufacturing a ferromagnetic core loaded with boric oxide. The method includes steps of performing pre-sintering on a mixture A comprising Fe<3>O<4>, manganese oxide, the boric oxide, zirconium fluoride, nickel oxide, borax, ferric oxide powder and aluminum powder and a mixture B comprising tantalum, titanium, tungsten, MoO<3>, Nb<2>O<5>, magnesium carbonate, lanthanum oxide and barium carbonate; sequentially performing grinding, mixing and pulping, powder spray-drying, green body pressing and sintering processes on the mixture A and the mixture B to obtain the ferromagnetic core. The total weight of the mixture B is equivalent to that of the mixture A. The method has the advantages that owing to an optimized formulation design and the sintering process, the initial permeability of a product manufactured by the method is 12500, cracking of the sintered product is little, the qualified rate of the product reaches 93.0% at least, the product is high in grain boundary resistivity and low in porosity, crystal grains of the product are large and uniform, the impendence characteristic of the product in a high-frequency range is excellent, various electromagnetic properties of the product are stable, and the ferromagnetic core product is applicable to various electronic fields.

The invention discloses a carbon-based ferrite magnetic core material for a transformer. The material comprises major ingredients and additives, wherein the major ingredients comprise 58 to 65.4 moles of Fe2O3, 16.3 to 21 moles of manganese oxide, 9.4 to 13 moles of zinc oxide, 1.2 to 2 moles of chromium oxide, 0.1 to 0.2 mole of ferrous disulfide, 0.6 to 1 mole of calcium oxide and 0.01 to 0.02 mole of rare earth composite magnetic-conducting powder according to a molar ratio; the additives comprise 100 to 200 parts per million of aluminum oxide, 60 to 100 parts per million of tin oxide and 50 to 70 parts per million of aluminum silicate based on the weight of the ferrite magnetic core material. The rare earth composite magnetic-conducting powder added to the ferrite magnetic core material has a magnetic energy product and stable magnetism, a preparation method is simple, and a finished product has the characteristics of high grain boundary resistivity, low porosity and large and uniform crystal grain sizes.

The invention discloses a HfO2-containing ferromagnetic core manufacturing method, which comprises the following steps of: proportioning 68-75 parts of reduced iron powder by weight, 15-17 parts of oxidized iron powder by weight, 4.2-4.5 parts of MnO by weight, 3.6-4.2 parts of ZnO by weight, 1.7-2.3 parts of modified tree ash by weight, 0.5-0.7 part of nano carbon by weight, 1-3 parts of HfO2 by weight, 2.5-2.7 parts of SiO2 by weight, 3.4-3.8 parts of V2O5 by weight and 2-3 parts of CuO by weight, and then sequentially conducting pre-sintering, primary ball milling, secondary ball milling, molding and sintering to obtain a HfO2-containing ferromagnetic core. The HfO2-containing ferromagnetic core manufacturing method has the advantages that the magnetic core formula is reasonable, the preparation method is simple, the saturation induction density of the manufactured magnetic core is higher, the loss is lower, the temperature resistance is higher, the added modified tree ash and the nano carbon can take a bridge bonding effect among different raw materials, the distribution of the used raw materials is better, the density is high, the crystal boundary resistivity is high, the porosity is low, the grains are large and uniform, the cracks are prevented from occurring during sintering, the texture is compact, the deformation is small, the raw material formula is reasonably improved, the deformation degree is small during sintering, and the magnetic core can be wire-cut, cut, ground and the like.

The invention discloses a tantalum-based ferrite magnetic core material used for transformer, which comprises a main material and an additive, the main material comprises the following components according to mol ratio: 57.1-64mol of Fe2O3, 16.2-20mol of manganese oxide, 10.1-15mol of zinc oxide, 4-5.2mol of copper oxide, 0.2-1 mol of zinc borate, 1-1.3mol of barium oxide and 0.01-0.02mol of rare earth composite magnetic conductive powder; and the additive comprises the following components according to weight ratio of the additive in the ferrite magnetic core material: 30-50ppm of aluminium triphosphate, 10-20ppm of titanium tetrachloride and 40-50ppm of silicon powder. The magnetic energy product of the rare earth composite magnetic conductive powder in the ferrite magnetic core material is high, and magnetic performance is stable, preparation method is simple, and the finished product has the characteristics of high crystal boundary resistivity, low porosity and large crystal grain.

The invention discloses a method for manufacturing a ferromagnetic core containing silicon dioxide. The method include steps of performing pre-sintering on a mixture A comprising Fe<2>O<3>, MoO, ZnO, aluminum nitride, copper, boron, aluminum, the silicon dioxide, titanium dioxide and tin and a mixture B comprising MoO<3>, V<2>O<5>, Bi<2>O<3>, boron dioxide, zirconium dioxide, barium dioxide, Ti and Ni; then sequentially performing grinding, mixing and pulping, powder spray-drying, green body pressing and sintering processes on the mixture A and the mixture B to obtain the ferromagnetic core. The method has the advantages that owing to an optimized formulation design and the sintering process, the initial permeability of a product manufactured by the method is 15000, cracking of the sintered product is little, the qualified rate of the product reaches 95% at least, the product is high in grain boundary resistivity and low in porosity, crystal grains of the product are large and uniform, the impendence characteristic of the product in a high-frequency range is excellent, various electromagnetic properties of the product are stable, and the ferromagnetic core product is applicable to various electronic fields.

The invention discloses a method for manufacturing a ferromagnetic core containing modified aluminum nitride. The method includes steps of performing pre-sintering on a mixture A comprising Fe<2>O<3>, MoO, ceramic powder, boron, titanium, aluminum hydroxide, the modified aluminum nitride and bentonite and a mixture B comprising SiO<2>, Nb<2>O<5>, yttrium oxide, tantalum oxide, Al, tin, vanadium and rubidium; sequentially performing grinding, mixing and pulping, powder spray-drying, green body pressing and sintering processes on the mixture A and the mixture B to obtain the ferromagnetic core. The total weight of the mixture B is equivalent to that of the mixture A. The method has the advantages that owing to an optimized formulation design and the sintering process, the initial permeability of a product manufactured by the method is 20000, cracking of the sintered product is little, the qualified rate of the product reaches 94.5% at least, the product is high in grain boundary resistivity and low in porosity, crystal grains of the product are large and uniform, the impendence characteristic of the product in a high-frequency range is excellent, various electromagnetic properties of the product are stable, and the ferromagnetic core product is applicable to various electronic fields.

The invention discloses a method for manufacturing a lithium-rich ferromagnetic core. The method includes steps of performing pre-sintering on a mixture A comprising Fe<3>O<4>, ZnO, lead tetroxide, zirconium fluoride, barium carbonate, lithium, palladium oxide and antimony trioxide and a mixture B comprising iron powder, Bi<2>O<3>, molybdenum, tungsten, gallium, zirconium oxide, chromium oxide and potassium oxide; sequentially performing grinding, mixing and pulping, powder spray-drying, green body pressing and sintering processes on the mixture A and the mixture B to obtain the lithium-rich ferromagnetic core. The total weight of the mixture B is equivalent to that of the mixture A. The method has the advantages that owing to an optimized formulation design and the sintering process, the initial permeability of a product manufactured by the method is 18800, cracking of the sintered product is little, the qualified rate of the product reaches 91.5% at least, the product is high in grain boundary resistivity and low in porosity, crystal grains of the product are large and uniform, the impendence characteristic of the product in a high-frequency range is excellent, various electromagnetic properties of the product are stable, and the ferromagnetic core product is applicable to various electronic fields.

The invention discloses a nickel-based ferrite magnetic core material for a transformer, which includes main materials and additives, and the main materials include: 57-63.6mol of Fe2O3, 17.0-22mol of manganese oxide, 10.2-16 mol of zinc oxide, 0.01-0.03 mol of stainless steel powder, 0.2-0.3 mol of barium sulfate, 0.01-0.02 mol of rare earth composite magnetically permeable powder; the additives include according to the weight ratio of the ferrite core material : Molybdenum powder of 80-90ppm, lithium nitride of 40-60ppm, magnesium hydroxide of 70-90ppm, the magnetic energy product of the rare earth composite magnetic conductive powder added to the ferrite magnetic core material of the present invention is high, magnetically stable, and the preparation method is simple , The finished product has the characteristics of high grain boundary resistivity, low porosity, large and uniform grains.

The invention discloses a method for manufacturing a ferromagnetic core loaded with boric oxide. The method includes steps of performing pre-sintering on a mixture A comprising Fe<3>O<4>, manganese oxide, the boric oxide, zirconium fluoride, nickel oxide, borax, ferric oxide powder and aluminum powder and a mixture B comprising tantalum, titanium, tungsten, MoO<3>, Nb<2>O<5>, magnesium carbonate, lanthanum oxide and barium carbonate; sequentially performing grinding, mixing and pulping, powder spray-drying, green body pressing and sintering processes on the mixture A and the mixture B to obtain the ferromagnetic core. The total weight of the mixture B is equivalent to that of the mixture A. The method has the advantages that owing to an optimized formulation design and the sintering process, the initial permeability of a product manufactured by the method is 12500, cracking of the sintered product is little, the qualified rate of the product reaches 93.0% at least, the product is high in grain boundary resistivity and low in porosity, crystal grains of the product are large and uniform, the impendence characteristic of the product in a high-frequency range is excellent, various electromagnetic properties of the product are stable, and the ferromagnetic core product is applicable to various electronic fields.

The invention discloses a method for manufacturing a ferromagnetic core containing modified nano-carbon. The method includes steps of performing pre-sintering on a mixture A comprising Fe<2>O<3>, MnO, ceramic powder, aluminum, zinc, niobium, the modified nano-carbon and straw ash and a mixture B comprising Bi<2>O<3>, CaCO<3>, nickel oxide, palladium oxide, scandium oxide, lanthanum oxide, Si and B; sequentially performing grinding, mixing and pulping, powder spray-drying, green body pressing and sintering processes on the mixture A and the mixture B to obtain the ferromagnetic core. The total weight of the mixture is equivalent to that of the mixture A. The method has the advantages that owing to an optimized formulation design and the sintering process, the initial permeability of a product manufactured by the method is 18000, cracking of the sintered product is little, the qualified rate of the product reaches 97% at least, the product is high in grain boundary resistivity and low in porosity, crystal grains of the product are large and uniform, the impendence characteristic of the product in a high-frequency range is excellent, various electromagnetic properties of the product are stable, and the ferromagnetic core product is applicable to various electronic fields.