Far-infrared ceramic material and manufacturing method thereof
A technology of far-infrared ceramics and a manufacturing method, which is applied in the field of ceramic materials, can solve the problems of unsatisfactory far-infrared radiation band and radiation efficiency, low thermal stability and the like, and achieves the effects of stable band, high thermal stability and high radiation efficiency.
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Embodiment 1
[0019] Weigh 860 grams of fused silica powder (amorphous silicon dioxide), 90 grams of crystalline zirconia powder, 30 grams of crystalline neodymium oxide, and 20 grams of crystalline europium oxide. Put the weighed raw materials into the ball mill together, add 1000 ml of deionized water, and ball mill until the maximum particle size reaches 2 microns, pour the ball milled slurry into the basin, put it in the oven for drying, and pulverize to obtain the powder . Add 100 grams of 3% PVA (polyvinyl alcohol) aqueous solution to the powder, stir evenly, briquetting, crushing, and passing through a 40-mesh sieve to obtain a granulated powder. The granulated powder is put into a mold of 80mm×120mm, and pressed under a pressure of 150 kg / cm2. After drying the formed body, put it into a high-temperature electric furnace, heat it at 1230° C. for 30 minutes and burn it, take it out after cooling, and obtain a far-infrared ceramic sample. The sample has a far-infrared emissivity of 0...
Embodiment 2
[0021] Weigh 480 grams of fused silica powder (amorphous silica), 350 grams of quartz powder (crystalline silica), 130 grams of zirconia, 10 grams of neodymium oxide, and 30 grams of europium oxide. Put the weighed raw materials into the ball mill together, add 800 ml of deionized water, and ball mill until the maximum particle size reaches 5 microns, then pour the ball milled slurry into the basin to adjust the moisture and fluidity of the slurry, and vacuum to eliminate air bubbles , to obtain the slurry for ceramic slip casting. Pour the ceramic grouting material into the gypsum mold and let it stand for a period of time. After the ceramic body is separated from the gypsum mold, the mold is demoulded, and the demoulded ceramic body is put into an oven for drying. Put the dried body into a high-temperature electric furnace, heat it at 1260° C. for 90 minutes and burn it, take it out after cooling, and obtain a far-infrared ceramic sample. In the wave band from 2.5 microns t...
Embodiment 3
[0023] Weigh 900 grams of fused silica powder (amorphous silica), 60 grams of crystalline zirconia powder, 30 grams of crystalline neodymium oxide, 10 grams of crystalline europium oxide, 20 grams of crystalline chromium chloride, and crystalline cobalt oxide 15 grams. Put the weighed raw materials into a ball mill, add 1200 ml of deionized water, and ball mill until the maximum particle size reaches 1.5 microns, pour the ball mill slurry into a basin, put it in an oven to dry, and crush to obtain ceramic powder body. Add 100 grams of 3% PVA aqueous solution to the ceramic powder, stir evenly, briquetting, crushing, and passing through a 40-mesh sieve to obtain a granulated powder. The granulated powder is put into a mold, and pressed under a pressure of 150 kg / cm2 to obtain a ceramic green body of 80mm×120mm×10mm. After drying the shaped green body, put it into a high-temperature electric furnace, heat it at 1200°C for 60 minutes for firing, take it out after cooling, and o...
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