Polylactic acid filter stick paper element and manufacturing method thereof
A technology of polylactic acid and paper core, which is applied in the direction of e-liquid filter element, single-component polyester artificial filament, melt spinning method, etc., which can solve the problem of low rod production rate, long curing time of filter rod, and difficulty in connecting cigarette sticks and other issues, to achieve the effects of saving forest resources and petroleum resources, good recycling and good biodegradability
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Embodiment 1
[0030] Example 1: The polylactic acid filter rod paper core is made from the following raw materials by melt spinning, in parts by weight: the ratio of levorotatory isomer: 95%; the melt index at 190°C under a load of 2.16 kg: 3.0g / 10 min; Intrinsic viscosity: 1.5; melting point: 173°C, 100 parts of polylactic acid with an average molecular weight of 330,000, 15 parts of tapioca starch, 0.10% by mass of substituted aryl phosphate lithium salt NA-03 in polylactic acid, and nano calcium carbonate in polylactic acid The mass percentage is: 0.15%.
[0031] Prepare as follows:
[0032] A. Raw material drying: vacuum dry the polylactic acid raw material at 75°C for 9 hours, so that the moisture content of the polylactic acid raw material is below 30ppm; Drying under temperature conditions for 5.5 hours; the dried polylactic acid and the nucleating agent are mixed uniformly to obtain a mixture;
[0033] B. Melt extrusion: Pour the mixture obtained in step A into the screw extrud...
Embodiment 2
[0041] Example 2: The polylactic acid filter rod paper core is made from the following raw materials by melt spinning, in parts by weight: the proportion of levorotatory is: 99%; at 190 ° C, the melt index under the load of 2.16 kg is: 2.0 g / 10 min; Intrinsic viscosity: 1.7; melting point: 165°C, 100 parts of polylactic acid with an average molecular weight of 330,000, 5 parts of a mixture of guar gum and potato starch, and the mass percentage of substituted aryl phosphate lithium salt NA-03 in polylactic acid is 0.20%. The mass percentage of nano-calcium carbonate in polylactic acid is: 0.1%.
[0042] Prepare as follows:
[0043] A. Raw material drying: vacuum dry the polylactic acid raw material at 75°C for 7 hours, so that the moisture content of the polylactic acid raw material is below 30ppm; Drying under temperature conditions for 4 hours; the dried polylactic acid and the nucleating agent are mixed uniformly to obtain a mixture;
[0044] B. Melt extrusion: Pour the...
Embodiment 3
[0052] Example 3: The polylactic acid filter rod paper core is made of the following raw materials by melt spinning, in parts by weight: the proportion of levorotatory is: 97%; at 190 ° C, the melt index under the load of 2.16 kg is: 4.0 g / 10 min; Intrinsic viscosity: 1.0; melting point: 170°C, 100 parts of polylactic acid with an average molecular weight of 330,000, 10 parts of tapioca starch, 0.30% by mass of substituted aryl phosphate lithium salt NA-03 in polylactic acid, and 0.30% by mass of nano calcium carbonate in polylactic acid The mass percentage is: 0.05%.
[0053] Prepare as follows:
[0054] A. Raw material drying: vacuum dry the polylactic acid raw material at 80°C for 8 hours, so that the moisture content of the polylactic acid raw material is below 30ppm; Drying under temperature conditions for 4 hours; the dried polylactic acid and the nucleating agent are mixed uniformly to obtain a mixture;
[0055] B. Melt extrusion: Pour the mixture obtained in step ...
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