Production method of lithium battery high-performance electrode material
An electrode material and manufacturing method technology, applied in battery electrodes, circuits, electrical components, etc., can solve the problems of battery gas swelling, easy gelling of the slurry, poor processing performance, etc., to reduce carbon content, good repeatability, The effect of improving processability
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Embodiment 1
[0019] A method for manufacturing a high-performance electrode material for a lithium battery, comprising the steps of:
[0020] (1) Multi-element precursor: According to the molar ratio of lithium, iron, and phosphorus elements of 4:1:1, lithium chloride, ferrous chloride, and phosphorus source compound are uniformly mixed with ammonium dihydrogen phosphate to obtain a mixture, and the mass of the mixture is added 0.02% boric acid and 0.06% glucose and citric acid are composed of an organic carbon source according to a weight ratio of 3:2 to obtain a precursor of a surface-coated carbon layer;
[0021] (2) Manufacture of pore agent sol: put ethanol in the container, turn on the thermostat, set the temperature at 50°C, control the speed at 50rpm, keep stirring for 15min, and mix the prepared multi-element precursor and ethanol according to the mass ratio of 1: 3 Dissolve in ethanol to form a sol, and add ammonia water to adjust the pH=4-5;
[0022] (3) Carbonization: After th...
Embodiment 2
[0025] A method for manufacturing a high-performance electrode material for a lithium battery, comprising the steps of:
[0026] (1) Multi-element precursor: According to the molar ratio of lithium, iron, and phosphorus elements 4:1:3, lithium chloride, ferrous chloride, and phosphorus source compound are uniformly mixed with diammonium hydrogen phosphate to obtain a mixture, and the mass of the mixture is added 0.03% boric acid and 0.08% glucose and citric acid are composed of an organic carbon source according to a weight ratio of 3:2 to obtain a precursor of a surface-coated carbon layer;
[0027] (2) Manufacture of pore agent sol: put ethanol in the container, turn on the thermostat, set the temperature at 50°C, control the speed at 60rpm, keep stirring for 10min, and mix the prepared multi-element precursor and ethanol at a mass ratio of 1: 3 Dissolve in ethanol to form a sol, and add ammonia water to adjust the pH=4-5;
[0028] (3) Carbonization: After the above sol eva...
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