Preparation method for surface light-emitting plastic optical fiber
A plastic optical fiber, whole body luminescence technology, applied in the direction of cladding optical fiber, optical waveguide light guide, optics, etc., can solve the problems of insufficient toughness, low optical fiber luminous intensity, complex manufacturing process, etc., to reduce production costs, expand application fields, and promote high value effect
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Embodiment 1
[0023] Embodiment 1: a kind of preparation method of whole body light-emitting type plastic optical fiber, comprises the following steps:
[0024] (1) Preparation of additives: Add 0.2 kg of rutile titanium dioxide powder with a particle size of 200 nm into a kneader with a volume of 1 L and add 20 g of polyoxyethylene sorbitan monooleate 83, start the kneader, and carry out Stir while raising the temperature to 65°C. Stir at 65°C for modification reaction for 30 minutes, stop heating; continue to stir and cool down to ambient temperature naturally, add the cooled product to a clean ball mill and grind until the particle size is 250 nm Get auxiliary agents left and right;
[0025] (2) Molding: Add 40 kg of polymethyl methacrylate pellets and additives to a kneader with a volume of 80 L; start the kneader and stir for 1.5 h, then use high-transparency polyethylene as the skin material, and add additives The core material is co-extruded on an extruder and drawn, cooled, and col...
Embodiment 2
[0027] Embodiment 2: A method for preparing a whole-body light-emitting plastic optical fiber, comprising the following steps:
[0028] (1) Auxiliary preparation: Mix the reflective material used as an additive with a surfactant to perform a modification reaction. After the modification is completed, cool the product and grind it to obtain the auxiliary agent;
[0029] (2) Forming: After the core material and the additives are evenly mixed, they are co-extruded and drawn with the skin material to obtain a filamentary optical fiber, which is the whole-body light-emitting plastic optical fiber.
[0030] The additive is a white powdery material that reflects light, and is a mixture of rutile-type titanium dioxide and anatase-type titanium dioxide; the particle size of the additive is 100-700 nm, and the polydispersity coefficient of the additive is less than 0.2. The particle size of the agent is 800-1200 nm.
[0031] Described tensio-active agent is the combination of polyoxyet...
Embodiment 3
[0035] Embodiment 3: A method for preparing a whole-body light-emitting plastic optical fiber, comprising the following steps:
[0036] (1) Auxiliary preparation: Mix the reflective material used as an additive with a surfactant to perform a modification reaction. After the modification is completed, cool the product and grind it to obtain the auxiliary agent;
[0037] (2) Forming: After the core material and the additives are evenly mixed, they are co-extruded and drawn with the skin material to obtain a filamentary optical fiber, which is the whole-body light-emitting plastic optical fiber.
[0038] The additive is a white powdery material that reflects light, and is a mixture of zinc oxide, calcium carbonate, and barium carbonate; the particle size of the additive is 700-1500 nm.
[0039] Described tensio-active agent is the combination of fatty alcohol polyoxyethylene ether sodium sulfate, Pingpingjia, and Turkish red oil, and its addition amount is 5% of additive by weigh...
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