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Reactive polymer for well drilling plugging and preparation method thereof

A polymer and drilling technology, applied in the field of polymers, can solve the problems of mutual separation of components, repeated leakage, and small water expansion of expansion plugging agent, so as to avoid detonation and gelation, improve performance, and aim at strong effect

Active Publication Date: 2016-10-26
CHINA PETROCHEMICAL CORP +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

During the entire period before the 1970s, high-viscosity drilling fluid plus bridge plugging materials (sawdust, mica, straw, mud balls, bricks, etc.) and cement plugs were mainly used. The plugging materials and methods were single, often resulting in Failure of lost circulation treatment
However, these existing lost circulation plugging materials usually have components separated from each other, unable to provide synergistic effect, and expansion plugging agent has small water expansion, and the plugging agent is not easy to stay stably under external force. Medium technical problems in the leakage layer, which may easily lead to poor plugging effect and repeated leakage after plugging

Method used

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  • Reactive polymer for well drilling plugging and preparation method thereof
  • Reactive polymer for well drilling plugging and preparation method thereof

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Embodiment 1

[0026] Gross weight of the present invention is 100g, and it is mainly formed by the raw material polymerization of following mass percent:

[0027] The first raw material is 62%, that is, 62g; the first raw material is acrylamide;

[0028] The second raw material is 37.5%, that is, 37.5g; the second raw material is hydroxyethyl methacrylate;

[0029] The initiator is 0.25%, that is, 0.25g; the initiator is an oxidizing agent, specifically sodium persulfate;

[0030] The reducing agent is 0.25%, that is, 0.25g; the reducing agent is sodium bisulfite.

[0031] The preparation method of the present invention comprises the following steps:

[0032] Step 1. Prepare each raw material according to the polymer formula quantity, and prepare dissolved water. The mass ratio of the polymer formula quantity to dissolved water is 1:2.5, that is, the water is 250g; prepare the reaction apparatus;

[0033] Step 2. Add the first raw material into the dissolved water, prepare an aqueous sol...

Embodiment 2

[0038] Gross weight of the present invention is 100g, and it is mainly formed by the raw material polymerization of following mass percent:

[0039] The first raw material is 67.5%, that is, 67.5g; the first raw material is a mixture of acrylamide and sodium acrylate, and the mass ratio of the two is 2:1;

[0040] The second raw material is 32%, i.e. 32g; the second raw material is hydroxyethyl acrylate;

[0041] The initiator is 0.35%, that is, 0.35g; the initiator is an oxidizing agent, specifically ammonium persulfate;

[0042] The reducing agent is 0.15%, that is, 0.15g; the reducing agent is sodium sulfite.

[0043] The preparation method of the present invention comprises the following steps:

[0044] Step 1. Prepare each raw material according to the polymer formula quantity, and prepare dissolved water. The mass ratio of the polymer formula quantity to the dissolved water is 1:3, that is, the water is 300g; prepare the reaction apparatus;

[0045] Step 2. Add the fi...

Embodiment 3

[0050] Gross weight of the present invention is 100g, and it is mainly formed by the raw material polymerization of following mass percent:

[0051] The first raw material is 80%, that is, 80g; the first raw material is a mixture of acrylamide, acrylic acid and sodium acrylate, and the mixing mass ratio of the three is 1:1:1;

[0052] The second raw material is 19%, that is, 19g; the second raw material is a mixture of hydroxyethyl acrylate, vinyl acetate and hydroxyethyl methacrylate, and the mixing mass ratio of the three is 1:1:1;

[0053] The initiator is 0.5%, that is, 0.5g; the initiator is an oxidizing agent, specifically ammonium persulfate;

[0054] The reducing agent is 0.5%, that is, 0.5g; the reducing agent is sodium bisulfite.

[0055] Preparation method of the present invention comprises the following steps:

[0056] Step 1. Prepare each raw material according to the polymer formula quantity, and prepare dissolved water. The mass ratio of the polymer formula quan...

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Abstract

The invention discloses a reactive polymer for well drilling plugging and a preparation method thereof. The polymer is mainly prepared by polymerizing the following raw materials in percentage by mass: 59-85% of first raw material, 14-40% of second raw material, 0.01-0.5% of initiator and 0.01-0.5% of reducer. The first raw material is one or mixture of more than two of acrylamide, acrylic acid and sodium acrylate. The second raw material is one or mixture of more than two of vinyl acetate, hydroxyethyl methacrylate and 2-hydroxyethyl acrylate. The method comprises the following steps: 1. preparing the raw materials and a solvent water; 2. after dissolving the first raw material, adding the second raw material; 3. adding the initiator, and continuously introducing nitrogen into the mixed solution to remove oxygen in the mixed solution; 4. in a nitrogen atmosphere, adding a reducer, heating the mixed solution to 20-40 DEG C, and carrying out polymerization reaction to obtain a jelly; and 5. drying the jelly, and pulverizing to obtain the polymer.

Description

technical field [0001] The invention relates to a polymer, in particular to a reactive polymer for oil and gas field drilling and plugging, and a preparation method of the polymer. Background technique [0002] Lost circulation is a complex problem in drilling operations. It causes drilling fluid to leak from the wellbore into the lost channel, which not only consumes a lot of mud and plugging materials, but also may cause well collapse, pipe sticking, blowout, and even lead to the scrapping of the wellbore, etc. Major accidents cause huge economic losses. Therefore, the plugging material is an indispensable substance in the process of leak prevention and plugging in drilling operations, and its performance will directly affect the success rate of plugging construction. [0003] In the 1960s, the country began to apply the plugging material to deal with lost circulation, and carried out some basic research work. During the entire period before the 1970s, high-viscosity dri...

Claims

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Application Information

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IPC IPC(8): C08F220/56C08F220/06C08F220/28C08F218/08C08F4/40C09K8/46
CPCC08F4/40C08F220/06C08F220/56C09K8/46C08F220/281C08F218/08
Inventor 杨国兴朱魁胡德云王权阳袁俊秀周成华逯贵广庞雨微王方博张珍李尧王大勇徐开模黄屋宇陈建君舒颖
Owner CHINA PETROCHEMICAL CORP
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