5results about How to "Prevent gelation" patented technology

This invention relates to the field of carbon nanotube technology, specifically disclosing a high-viscosity carbon nanotube conductive paste and its preparation method. The raw materials for this high-viscosity carbon nanotube conductive paste include ultra-long single-walled carbon nanotubes, short-cut multi-walled carbon nanotubes, conductive carbon black, carboxyl-terminated hyperbranched polyester-polyethylene glycol block copolymer, polyacrylic acid, fluorinated silane coupling agent, γ-butyrolactone, and N-methylpyrrolidone. The high-viscosity carbon nanotube conductive paste provided by this invention achieves uniform dispersion, low volume resistivity, excellent anti-settling properties, and good coating processability of the carbon nanotube conductive paste under high solids content through the synergistic effect of the carboxyl-terminated hyperbranched polyester-polyethylene glycol block copolymer, the fluorinated silane coupling agent, and polyacrylic acid, combined with multi-stage grinding and high-pressure homogenization processes.

The invention relates to light dehydrofluorination modified PVDF (polyvinylidene fluoride) resin as well as a preparation method and application thereof. The preparation method comprises the following steps: dissolving PVDF resin to be modified in a polar solvent to obtain a PVDF solution; the method comprises the following steps: adding weak organic alkali into a PVDF solution in a protective gas atmosphere, and then carrying out dehydrofluorination modification; and after the reaction is finished, terminating the reaction by using an acidic alcohol solution, and carrying out precipitation, washing and drying to obtain the light dehydrofluorination modified PVDF resin. Compared with the prior art, the high-temperature-resistant PVDF resin with high thermal stability and good melt processability can be obtained, and the high-temperature-resistant PVDF resin can be used for 200-DEG C-grade injection molding or extrusion molding products.

The invention discloses a preparation method of high-solid-content and high-flowability sodium ion aqueous positive electrode slurry, which comprises the following steps: S1, preparation of a glue solution: adding a binder into deionized water, and stirring to obtain the glue solution; s2, preparation of a high-fluidity glue solution: adding a first glue solution flow regulator into the glue solution, and stirring at a high speed to obtain the high-fluidity glue solution; s3, preparing a weakly alkaline glue solution, namely adding a second pH flow regulator into the high-flowability glue solution, and stirring to obtain the weakly alkaline glue solution; s4, preparation of a conductive adhesive solution: adding a first conductive agent into the alkalescent adhesive solution, and stirring to obtain the conductive adhesive solution; s5, preparation of first slurry: adding the active substance material into the conductive adhesive solution in batches, stirring and dispersing, and adjusting the viscosity to obtain the first slurry; and S6, preparation of finished slurry: adding the second conductive agent into the first slurry, and stirring and dispersing at a medium-low speed to obtain the final slurry. The invention has the characteristics of good fluidity, high solid content and green and environment-friendly process.

The invention discloses a preparation method and application of an organic silicon modified aluminum-zirconium / titanium bimetallic composite fluorine removal agent (CSAZ / CSAT), and belongs to the technical field of water treatment. Zirconium tetrachloride or diluted titanium tetrachloride is compounded with aluminum chloride to construct a bimetallic framework. Meanwhile, vinyltriethoxysilane (VTES) is introduced as an organic modifier, and heterogeneous copolymerization is carried out on an organic silicon hydrolysate and metal hydroxyl by controlling the dripping rate and the reaction temperature. According to the fluorine removal agent, by utilizing the bridging effect of organic silicon and the synergistic effect of double metals, the adsorption, complexation and net capture capacities on fluorine ions are remarkably enhanced. Experiments show that when the molar ratio of Al to Zr is 9: 1 (CSAZ) or the molar ratio of Al to Ti is 14: 1 (CSAT), the defluorination effect is optimal. When the agent is applied, the pH value does not need to be adjusted, a coagulant aid does not need to be added, efficient removal of fluorine ions can be achieved only through a single agent, the agent has the advantages of being low in dosage, neutral in effluent pH value and the like, and the industrial problems that a traditional fluorine removal process is long in process, large in acid and alkali consumption and difficult in sludge treatment are effectively solved.

The application belongs to the technical field of haematococcus pluvialis separation, and specifically discloses a ternary cross-linked nanofiltration membrane, a preparation method and application. The nanofiltration membrane comprises a polyethersulfone ultrafiltration membrane base film, a polydopamine intermediate layer and a ternary cross-linked functional layer sequentially loaded on the surface of the polyethersulfone ultrafiltration membrane base film. The preparation method comprises the following steps: preparing the polydopamine intermediate layer, anchoring oxidized haematococcus pluvialis polysaccharide, covalently cross-linking polyphenylated chitosan, coordination cross-linking iron ions, and post-treatment to obtain the ternary cross-linked nanofiltration membrane. The ternary cross-linked nanofiltration membrane is used for separating haematococcus pluvialis polysaccharide and astaxanthin ester. The ternary cross-linked functional layer simultaneously has three separation abilities of size screening, charge regulation and coordination selection, realizes selective separation of astaxanthin ester and neutral oil with similar molecular weights, and effectively retains macromolecular polysaccharide.