High-efficiency environment-friendly LED chip cleaning agent and application method

A technology of LED chips and cleaning agents, applied in detergent compositions, detergent compounding agents, chemical instruments and methods, etc., can solve problems such as environmental hazards, human injury, and increased production costs, and achieve strong wetting ability and prevent Effects of secondary pollution or corrosion

Active Publication Date: 2017-01-25
ZHEJIANG AUFIRST MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The strong acid cleaning effect is good, but it is harmful to the human body and seriously pollutes the environment. It needs special treatment before it can be discharged.
Chinese Invention Patent Application Publication CN101661869 discloses a gallium arsenide wafer cleaning method after polishing. The main process steps are concentrated sulfuric acid cleaning and strong alkali cleaning, which can effectively clean wax spots, dust, and dirty spots on the wafer surface. The acid and lye used are harmful to the environment and human body, and special treatment is required during the discharge process, which increases the production cost
Chinese Invention Patent Application Publication CN102703238 discloses a wax removal cleaning agent, the main component of which contains a large amount of phosphate, which will cause eutrophication of the water body and cause environmental hazards if discharged into the river water

Method used

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  • High-efficiency environment-friendly LED chip cleaning agent and application method
  • High-efficiency environment-friendly LED chip cleaning agent and application method
  • High-efficiency environment-friendly LED chip cleaning agent and application method

Examples

Experimental program
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Effect test

preparation example Construction

[0031] The preparation method of the product in the embodiment 1-8 is: add a certain amount of ultrapure water in the reactor, start to stir; add acetylenic glycol surfactant by mass ratio, stir for 3-5 minutes; add fluorine by mass ratio Carbon surfactant, stir for 3-5 minutes; add imidazoline amphoteric surfactant according to mass ratio, stir for 5 minutes; add emulsifier according to mass ratio, stir for 5 minutes; add corrosion inhibitor according to mass ratio, stir for 5 minutes ; Add a chelating agent according to the mass ratio and stir for 5 minutes; finally add a solubilizer and stir for 20 minutes until it is transparent, and the LED chip cleaning agent is obtained.

[0032] The percentages in the examples are percentages by weight unless otherwise specified. The following methods are used to test the effect of the following cleaning agents: make an aqueous solution according to the concentration of 10%, and clean the workpiece by ultrasonic at 70°C, and the cleani...

Embodiment 9

[0036] Take a 1kg product as an example, add 67.5% ultrapure water into the reaction kettle, start stirring; then add 5% of 2,4,7,9-tetramethyl-5-decyne-4,7diol 30% ethylene oxide, stirred for 3 minutes; then added 2% tripolyepoxyhexafluoropropane amido betaine, stirred for 5 minutes; then added 3% aminoethyl amphoteric imidazoline, stirred for 3 minutes; then added 15 % triethanolamine oleate, stirred for 3 minutes; then added 1.5% urotropine, stirred for 3 minutes; then added 2% nitrilotriacetic acid, stirred for 3 minutes; then added 4% alkyl glucoside, stirred for 15 minutes to transparent. The resulting product has a good cleaning effect.

[0037] The LED chip cleaning agent in this embodiment is made by mixing the ingredients in the following table.

[0038]

Embodiment 10

[0040] Adopt the method among the embodiment 9, what the components in the following table are mixed to cleaning agent product. The cleaning effect of this product is compared with the cleaning effect of the product in Example 8 figure 2 .

[0041]

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Abstract

The invention relates to a high-efficiency environment-friendly LED chip cleaning agent and an application method, belonging to the field of electronic cleaning of photoelectron devices. The cleaning agent is prepared from the following components by weight percent: 1 to 10 percent of alkynediols surfactants, 0.1 to 5 percent of fluorocarbon surfactants, 2 to 10 percent of imidazoline ampholytic surfactants, 3 to 20 percent of emulsifiers, 0.5 to 5 percent of corrosion inhibitors, 1 to 5 percent of chelating agents, 1 to 5 percent of solubilizers, and 40 to 91.8 percent of ultrapure water. The cleaning agent contains the alkynediols surfactants, so that the moisturizing capacity is extremely high, and dirt such as polishing wax, grinding cream and the like on the surface of a chip can be rapidly stripped and dissolved. The cleaning agent contains the imidazoliine ampholytic surfactants, so that a layer of molecular film can be formed on the surface of the chip so as to protect the surface of a chip electrode, and to prevent the electrode from being secondarily polluted or corroded. The cleaning agent is mainly used for cleaning residues such as the polishing wax, the grinding cream, organic contaminants, solid particles and the like, on the surface of the polished LED chip, contains no phosphate, and can completely substitute the existing acid pickling process. The cleaning agent is also suitable for cleaning other workpieces.

Description

technical field [0001] The invention relates to a high-efficiency and environment-friendly LED chip cleaning agent and a use method thereof, which belong to the field of electronic cleaning of optoelectronic devices. Background technique [0002] LED chips are the core components of LED lights, and their main function is to convert electrical energy into light energy. The manufacturing process of LED chips includes grinding, polishing, etching, evaporation, cutting, cleaning and other processes. For chips used in device manufacturing and integrated circuit manufacturing, chemical mechanical polishing technology is generally used to smooth the chip surface. In the polishing process of the chip, due to the thin thickness of the chip, the commonly used polishing method is wax polishing. Wax polishing is to completely fix the chip on the substrate, and it is not easy to break during the polishing process. This is the main polishing method at present. After the chip is polishe...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11D1/94C11D3/20C11D3/26C11D3/33C11D3/60C11D3/28H01L21/02
CPCC11D1/004C11D1/008C11D1/22C11D1/662C11D1/667C11D1/721C11D1/74C11D1/94C11D3/2086C11D3/26C11D3/28C11D3/33H01L21/02057H01L21/02082
Inventor 李波侯军褚雨露
Owner ZHEJIANG AUFIRST MATERIAL TECH CO LTD
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