A kind of preparation method of carbon fiber surface deposition molybdate nanomaterial
A carbon fiber material, surface deposition technology, applied in nanotechnology, nanotechnology, nanotechnology and other directions for materials and surface science, can solve problems such as high cost and complex operation, achieve small investment, simple processing, mild reaction conditions Effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0030] The present invention provides a preparation method for depositing molybdate nanomaterials on the surface of carbon fibers, comprising the following steps: 1) degreasing and surface cleaning treatment of carbon fibers: carbon fibers are first soaked in acetone for 1-3 hours, and cleaned with deionized water After cleaning, place it in a tube furnace with a nitrogen protection temperature of 350-450° C. for 15-60 minutes. 2) Anode treatment: polish the anode soluble metal sheet with sandpaper, then place it in acetone for degreasing treatment, then rinse it with deionized water, dry the metal sheet with nitrogen air flow, and use the carbon fiber material of the above step 1 with The self-made clip is attached to the surface of the metal sheet to make a simple anode, and the carbon fiber material is carbon felt or carbon cloth. 3) Carbon fiber surface electrodeposition: After the above treatment, in the attached Figure 1a Carry out electrolysis in the shown cationic mem...
Embodiment 1
[0036] 1) Use the carbon felt close to the iron sheet as a whole as the anode, use the inert electrode as the cathode, use 90ml of sodium molybdate aqueous solution containing depolarizer as the anolyte, use 90ml of dilute hydrochloric acid solution as the catholyte, and use the cationic membrane as the diaphragm In the double-chamber electrolytic cell, the temperature is controlled at 70-80°C, and the electrolysis is carried out by constant current electrolysis for 5 minutes; in the anolyte, the concentration of sodium molybdate is 0.1mol / L; the concentration of depolarizer is 0.01mol / L ; The depolarizer is sodium chloride; the cationic membrane is Nafion perfluorosulfonic acid 212 type cation exchange membrane; the concentration of acid solution is 0.1mol / L; the current of constant current electrolysis is 0.6A, and the current density is 0.086A / cm 2 ;
[0037] 2) After the electrolysis is completed, dry the obtained anode, remove the carbon felt, wash the obtained carbon fel...
Embodiment 2
[0039] 1) Use the carbon felt close to the iron sheet as a whole as the anode, use the inert electrode as the cathode, use 90ml of sodium molybdate aqueous solution containing depolarizer as the anolyte, use 90ml of dilute hydrochloric acid solution as the catholyte, and use the cationic membrane as the diaphragm In the double-chamber electrolyzer, the temperature is controlled at 60-70°C, and the electrolysis is carried out by constant current electrolysis for 5 minutes; in the anolyte, the concentration of sodium molybdate is 0.1mol / L; the concentration of depolarizer is 0.01mol / L ; The depolarizer is sodium chloride; the cationic membrane is Nafion perfluorosulfonic acid 212 type cation exchange membrane; the concentration of acid solution is 0.1mol / L; the current of constant current electrolysis is 0.3A, and the current density is 0.06A / cm 2 ;
[0040] 2) After the electrolysis is completed, dry the obtained anode, remove the carbon felt, wash the obtained carbon felt and ...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More