Antibacterial cotton textile fiber preparation method

A cotton textile, antibacterial technology, applied in the field of preparation of enhanced textile antibacterial, to achieve a long-lasting antibacterial effect

Active Publication Date: 2017-02-22
安徽富颍纺织科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These antibacterial agents have their own characteristics, but it is difficult to meet the basic conditio

Method used

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  • Antibacterial cotton textile fiber preparation method

Examples

Experimental program
Comparison scheme
Effect test

example 1

[0023] (1) Catalyst A: Weigh 30g of powdered γ-Al 2 o 3 , 5g of vinylsilazane, 0.7g of adipic acid, 0.6g of ethylenediaminetetraacetic acid, add 300ml of deionized water, react at 75°C for 2h, then add 0.6g of hydroxyethylethylenediaminetriacetic acid, 70 React at ℃ for 1 hour, then add 0.3 g of triethanolamine, react at 60 ℃ for 1 hour, let stand for 0.5 hours, dry at 110 ℃ for 18 hours, take a 20-mesh sample as the required catalyst A after tableting, crushing and sieving;

[0024] (2) Preparation of Coptidis Rhizoma Extract: Dissolve 80 g of crushed Coptidis Rhizoma powder in 400 mL of deionized water, add 1.3 g of catalyst A prepared in (1) above, 0.8 g of acetyl tributyl citrate and butyl carbitol Heat 0.3 g at 100°C for 60 minutes, filter while it is hot, concentrate the filtrate by distillation under reduced pressure, and dry the concentrate in a vacuum dryer at 60°C to obtain Coptidis Rhizoma extract;

[0025] (3) Preparation of crosslinking agent: Take 8g of cornsta...

example 2

[0029] (1) Catalyst A: Weigh 30g of powdered γ-Al2O3, 5g of vinylsilazane, 0.7g of adipic acid, and 0.6g of ethylenediaminetetraacetic acid, add 300ml of deionized water, and react at 75°C 2h, then add 0.6g of hydroxyethyl ethylenediamine triacetic acid, react at 70°C for 1h, then add 0.3g of triethanolamine borate, react at 60°C for 1h, let stand for 0.5h, dry at 110°C for 18h, press into tablets, crush , After sieving, take a 50-mesh sample as catalyst A;

[0030] (2) Preparation of Coptidis Rhizoma Extract: Dissolve 80 g of crushed Coptidis Rhizoma powder in 400 mL of deionized water, add 1.3 g of the catalyst A prepared in (1) above, 0.8 g of acetyl tributyl citrate and 0.3 g of alcohol ether glycoside AEG g, keep warm at 100°C for 60min, filter while it is hot, concentrate the filtrate by distillation under reduced pressure, and dry the concentrated solution in a vacuum dryer at 60°C to obtain the extract of Coptis rhizome;

[0031] (3) Preparation of cross-linking agent...

example 3

[0035] (1) Catalyst A: Weigh 30g of powdered γ-Al2O3, 5g of vinylsilazane, 0.7g of adipic acid, and 0.6g of ethylenediaminetetraacetic acid, add 300ml of deionized water, and react at 75°C 2h, then add 0.6g of hydroxyethylethylenediaminetriacetic acid, react at 70°C for 1h, then add 0.3g of oleic acid diethanolamide, react at 60°C for 1h, let stand for 0.5h, dry at 110°C for 18h, press into tablets and crush , After sieving, take a 40-mesh sample as catalyst A;

[0036] (2) Preparation of Coptis chinensis extract: Dissolve 80 g of crushed Coptis chinensis powder in 400 mL of deionized water, add 1.3 g of the catalyst A prepared in (1), 0.8 g of acetyl tributyl citrate and N-chlorosuccinate Incubate 0.3 g of imide at 100°C for 60 minutes, filter while it is hot, concentrate the filtrate by distillation under reduced pressure, and dry the concentrated solution in a vacuum dryer at 60°C to obtain the extract of Coptis chinensis;

[0037] (3) Preparation of crosslinking agent: Ta...

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Abstract

The invention discloses an antibacterial cotton textile fiber preparation method, which is characterized by comprising: immersing 5 g of a fabric in a caustic soda solution with a mass fraction of 5-30% for 15-60 min at a temperature of 20-35 DEG C, taking out the fabric, placing into 100 g of a chloroacetic acid aqueous solution with a mass concentration of 10%, taking out after 30-45 min, sealing the fabric in a polyethylene plastic bag, placing in a 30-80 DEG C oven, carrying out a reaction for 1-3 h, washing 3-5 times with 50 ml of an ethanol and water mixing solution with a volume ratio of 80:20, drying, dispersing 0.6 g of sodium alginate, 0.7 g of chitosan and 2.2 g of a coptis chinensis extract in 10 g of distilled water, carrying out mixing stirring for 15 min at a temperature of 30 DEG C to obtain the chitosan solution of microcapsule, immersing the modified cotton textile fiber in the chitosan solution of the microcapsule for 30-45 min, taking out, immersing 6 g of a modified starch cross-linking agent, carrying out a reaction for 0.5-1.5 h, adding 0.3 g of a material C, carrying out a reaction for 1 h at a temperature of 90 DEG C, drying for 5-15 min at a temperature of 150 DEG C, carrying out water washing 3-5 times, and drying so as to obtain the antibacterial textile. The prepared textile of the present invention has the lasting antibacterial effect.

Description

technical field [0001] The invention relates to a preparation method for enhancing textile antibacterial properties, in particular to a preparation method for antibacterial cotton textile fibers. Background technique [0002] Coptis chinensis is the dry rhizome of Coptis chinensis, Coptis triangularis or Yunlian, also known as Chuanlian and chicken feet. This taste is bitter, cold in nature, the heart, stomach, liver, and large intestine meridians, and has the effects of clearing away heat, purging fire, drying dampness, and detoxifying. Clinically, it is mostly used to treat dysentery, acute gastroenteritis, chronic diarrhea, respiratory infection and various inflammations. In recent years, studies have found that it also has obvious effects in anti-tumor, anti-arrhythmia, and hypoglycemia. [0003] The main components are alkaloids and lignans, in addition to phenolic acids, volatile oils, flavonoids, coumarins, terpenes, steroids, polysaccharides, etc. The alkaloids fou...

Claims

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Application Information

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IPC IPC(8): D06M15/03D06M15/11D06M15/13D06M13/00D06M23/12B01J31/26
CPCB01J31/26D06M13/00D06M15/03D06M15/11D06M15/13D06M23/12D06M2101/06
Inventor 唐雪平耿頔杨欣
Owner 安徽富颍纺织科技股份有限公司
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