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Impact resistant rubber material and preparation method thereof

A rubber material and impact-resistant technology, which is applied in the field of impact-resistant rubber materials and its preparation, can solve the problems of low comprehensive performance of graphene oxide/polymer composite materials, easy agglomeration of graphene oxide, uneven dispersion, etc. , to achieve the effects of improving thermal stability and mechanical properties, enhancing water solubility, and improving emulsifying ability

Inactive Publication Date: 2017-04-05
曾庆明
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, at present, the functionalization method of graphene is not very mature and needs to be further improved. In order to realize its industrialization, in-depth research is needed, especially how to use covalent and non-covalent bond modification methods to have special structures and properties. Combining chemical molecules with graphene to give full play to the advantages of both is the focus of current research; it has been found that the main problem in the process of preparing graphene oxide / polymer composites is that graphene oxide is easy to agglomerate, and in The dispersion in the polymer is not uniform, and the bonding interface between graphene oxide and polymer is not good, which ultimately leads to the low comprehensive performance of graphene oxide / polymer composites, which limits its further industrial application.

Method used

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Embodiment Construction

[0019] A kind of impact-resistant rubber material, it is made up of the following raw materials of weight part:

[0020] Antiaging agent RD4, talcum powder 18, aluminum tripolyphosphate 1, dioctyl azelate 18, accelerator DM2, graphene oxide 10, sodium borohydride 1, p-aminobenzenesulfonic acid 3, 0.8mol / l hydrochloric acid 14, Sodium nitrite 1, styrene 43, potassium persulfate 0.3, hydrazine hydrate 0.5, butadiene rubber 210, vulcanizing agent MOCA1.7, tributyltin trichloride 2, magnesium stearate 4, ammonium metaborate 3, β Hydroxyalkylamide 1, Polytetrafluoroethylene 2, Cyclohexanehexanol 1, Gamma Aminopropyltriethoxysilane 1.7.

[0021] A preparation method of the impact-resistant rubber material, comprising the following steps:

[0022] (1) Add graphene oxide to deionized water 900 times its weight, and ultrasonicate for 27 minutes to obtain a graphene suspension;

[0023] (2) Add the above-mentioned aluminum tripolyphosphate into deionized water 10 times its weight, sti...

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PUM

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Abstract

The invention discloses an impact resistant rubber material. The impact resistant rubber material comprises the following raw materials in parts by weight: 4 to 6 parts of an anti-aging agent RD, 18 to 20 parts of talcum powder, 1 to 2 parts of aluminium triphosphate, 18 to 20 parts of dioctyl azelate, 2 to 3 parts of an accelerant DM, 10 to 14 parts of graphene oxide, 1 to 2 parts of sodium borohydride, 3 to 4 parts of sulfanilic acid, 14 to 20 parts of hydrochloric acid of which the concentration is 0.8 mol / l to 1 mol / l, 1 to 2 parts of sodium nitrite, 43 to 50 parts of styrene, 0.3 to 0.5 part of potassium persulfate, 0.5 to 1 part of hydrazine hydrate, 210 to 300 parts of butadiene rubber, 1.7 to 2 parts of a vulcanizing agent MOCA, 2 to 3 parts of tributyl tin chloride, 4 to 7 parts of magnesium stearate, 3 to 4 parts of ammonium metaborate, 1 to 2 parts of beta-hydroxyalkylamide, 2 to 3 parts of polytetrafluoroethylene, 1 to 2 parts of inositol and 1.7 to 2 parts of gamma-aminopropyltriethoxysilane. The rubber material is high in surface strength and good in toughness, and has quite good impact resistance.

Description

technical field [0001] The invention relates to the technical field of rubber materials, in particular to an impact-resistant rubber material and a preparation method thereof. Background technique [0002] Graphene-based polymer nanocomposites are considered to be the most promising fields for graphene applications. The main reason is that on the one hand, the products of polymer materials play an increasingly important role in people's lives, and have surpassed inorganic non-metallic materials and metal materials to become the most used materials in people's lives; on the other hand, graphene and Its derivatives, blackene oxides, each have a unique two-dimensional structure and excellent performance, and are ideal fillers. Currently, there are three main preparation methods for the preparation of graphene / polymer composites: flame-melt blending, solution blending, and in-situ polymerization. These three methods have their own advantages and disadvantages: melt blending ca...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L9/00C08L25/06C08K13/06C08K9/04C08K3/04C08K3/32C08K5/098C08K5/11C08K3/34
CPCC08L9/00C08K2201/011C08L2201/08C08L2205/03
Inventor 曾庆明
Owner 曾庆明
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