A kind of rapid prototyping material for three-dimensional printing and its preparation method
A technology for 3D printing and molding materials, applied in the field of 3D printing, can solve the problems of affecting the efficiency of rapid prototyping of 3DP technology, the accuracy of printed parts, the difficulty of ensuring the accuracy of printed parts, and the slow hardening speed of gypsum powder. The processing process, the use method is simple, and the effect is conducive to market promotion
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Embodiment 1
[0033] Weigh 800g gypsum powder (commercially available α-calcium sulfate hemihydrate, product average particle size 65µm, whiteness 93%, initial setting time 6.5min, 3h flexural strength 5.5MPa), 150g gellan gum powder, 15g gas phase dioxide Mix the silicon powder evenly, ball mill for 4 hours at room temperature, then add 35g of sodium alginate (of which β - D -mannuronic acid unit with α - L - The molar ratio of guluronic acid units is 0.35) mixed ball mill for 2 hours, and passed through a 180-mesh sieve to obtain a modified gypsum-based powder material modified with sodium alginate, with a particle size range of 1-80 µm and a bulk density of 0.98 g / cm 3 , real density 2.80g / cm 3 , powder flow rate 5.5g / s, hardening speed 80s.
[0034] Prepare a 0.2mol / L calcium chloride solution as an aqueous binder.
[0035] Take the above-mentioned modified gypsum-based powder material and water-based adhesive liquid, and conduct a machine test on the PJ660 rapid prototyping printe...
Embodiment 2
[0038] Weigh 850g gypsum powder (commercially available α-calcium sulfate hemihydrate, average particle size 80µm, whiteness 92%, initial setting time 7min, 3h flexural strength 6.5MPa), 120g agarose gel powder, 10g gas phase dioxide Mix the silicon powder evenly, ball mill for 6 hours at room temperature, then add 20g of sodium alginate (of which β - D -mannuronic acid unit withα - L - The molar ratio of guluronic acid units is 0.85) mixed with ball mill for 1 hour, and passed through a 180-mesh sieve to obtain a modified gypsum-based powder material modified with sodium alginate, with a particle size range of 1-80 µm and a bulk density of 1.09 g / cm 3 , real density 3.02g / cm 3 , powder flow rate 5.3g / s, hardening speed 90s.
[0039] Prepare a 0.2mol / L zinc chloride solution as an aqueous binder.
[0040] Take the above-mentioned modified gypsum-based powder material and water-based adhesive liquid, and carry out the machine test on the PJ660 rapid prototyping printer prod...
Embodiment 3
[0043] Weigh 750g gypsum powder (commercially available α-calcium sulfate hemihydrate, product average particle size 80µm, whiteness 92%, initial setting time 7min, 3h flexural strength 6.5MPa), 150g cardlan gum powder, 10g gas phase dioxide Mix the silicon powder evenly, ball mill for 6 hours at room temperature, then add 90g of sodium alginate (of which β - D -mannuronic acid unit with α - L - The molar ratio of guluronic acid units is 1.05) mixed ball mill for 3 hours, and passed through a 180-mesh sieve to obtain a modified gypsum-based powder material modified with sodium alginate, with a particle size range of 1-80 µm and a bulk density of 0.91 g / cm 3 , the real density is 2.73g / cm 3 , The powder flow rate is 4.3g / s, and the hardening speed is 65s.
[0044] Prepare a 0.3mol / L aluminum chloride solution as an aqueous binder.
[0045] Take the above-mentioned modified gypsum-based powder material and water-based adhesive liquid, and carry out the machine test on the P...
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