Liquid porous material for extracting methane as well as preparation method and application thereof
A porous material and liquid technology, applied in the field of landfill gas purification and concentration, can solve problems such as fire, environmental pollution, and danger, and achieve the effect of less energy consumption and simple method
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Embodiment 1
[0026] A method for preparing a liquid porous material for extracting methane, comprising the following steps:
[0027] (1) Under a nitrogen atmosphere, react the mixture I prepared by 1.5g of 2,3-O-isopropylidene-D-threol, 4g of sodium hydride, and 500mL of 1,4-dioxane at 60°C 1.5h, then add the mixed solution II prepared by tetraethylene glycol di-p-toluenesulfonate 4g and 1,4-dioxane 250mL, the mass ratio of mixed solution I to mixed solution II is 1.99:1, in Reaction at 90°C for 23 hours to obtain the product S1, the product S1 was extracted with chloroform and water, the chloroform layer (lower layer) was dried and dehydrated with sodium sulfate, and then concentrated in vacuo;
[0028] (2) Add 5 g of the concentrated product S1 to 5 mL of 2mol / L hydrochloric acid and 17 mL of methanol and react at room temperature for 18 hours to obtain the product S2. The product S2 is extracted with saturated sodium bicarbonate solution and chloroform, and the chloroform layer (lower l...
Embodiment 2
[0045] A method for preparing a liquid porous material for extracting methane, comprising the following steps:
[0046] (1) Under a nitrogen atmosphere, react 1.5g of 2,3-O-isopropylidene-D-threol with 4g of sodium hydride and 490mL of 1,4-dioxane at 70°C for 1h, then add four The mixed solution II prepared by 4 g of ethylene glycol di-p-toluenesulfonate and 260 mL of 1,4-dioxane, the mass ratio of the mixed solution I to the mixed solution II is 1.77, reacted at 100 ° C for 22 hours to obtain the product S1, the product S1 was extracted with chloroform and water, the chloroform layer (lower layer) was dried and dehydrated with sodium sulfate, concentrated in vacuo, and purified by column chromatography;
[0047] (2) Add 5 g of the purified product S1 to 10 mL of 3 mol / L hydrochloric acid and 17 mL of methanol to react at room temperature for 20 hours to obtain the product S2. The product S2 is extracted with saturated sodium bicarbonate solution and chloroform, and the chloro...
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