A kind of preparation method of aluminum-based graphene, carbon nanotube composite heat dissipation material
A carbon nanotube composite and heat-dissipating material technology, applied in heat exchange materials, chemical instruments and methods, electrolytic coatings, etc. , Improve heat dissipation efficiency and prolong service life
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Embodiment 1
[0021] A preparation method of aluminum-based graphene and carbon nanotube composite heat dissipation material, characterized in that it comprises the following steps:
[0022] (1) put into the same amount of graphene powder and carbon nanotube respectively in dehydrated ethanol solution, be made into the mixed solution that concentration is 0.02mg / ml graphene, carbon nanotube, then add aluminum salt solution, be made into The mixed solution of aluminum salt graphene and carbon nanotubes with an aluminum salt concentration of 0.6 mg / ml is dispersed by ultrasonic waves for 3 hours to obtain a mixed electrophoretic solution of uniformly dispersed aluminum salt graphene and carbon nanotubes;
[0023] (2) Ultrasound an aluminum sheet with a thickness of 0.01 mm in absolute ethanol solution for 10 minutes, then soak it in 5% dilute nitric acid for 0.5 min, rinse it with deionized water several times, and use it as the cathode after drying;
[0024] (3) With the graphite sheet equiv...
Embodiment 2
[0030] A preparation method of aluminum-based graphene and carbon nanotube composite heat dissipation material, characterized in that it comprises the following steps:
[0031] (1) put into the same amount of graphene powder and carbon nanotube respectively in dehydrated ethanol solution, be made into the mixed solution that concentration is 0.08mg / ml graphene, carbon nanotube, then add aluminum salt solution, be made into The mixed solution of aluminum salt graphene and carbon nanotubes with an aluminum salt concentration of 0.4 mg / ml is dispersed by ultrasonic waves for 5 hours to obtain a mixed electrophoretic solution of uniformly dispersed aluminum salt graphene and carbon nanotubes;
[0032] (2) Ultrasonicate an aluminum sheet with a thickness of 0.05 mm in absolute ethanol solution for 8 minutes, then soak it in 8% dilute nitric acid for 1 minute, rinse it with deionized water several times, and use it as the cathode after drying;
[0033] (3) With the graphite sheet eq...
Embodiment 3
[0039] A preparation method of aluminum-based graphene and carbon nanotube composite heat dissipation material, characterized in that it comprises the following steps:
[0040] (1) put into the same amount of graphene powder and carbon nanotube respectively in dehydrated ethanol solution, be made into the mixed solution that concentration is 0.1mg / ml graphene, carbon nanotube, then add aluminum salt solution, be made into The mixed solution of aluminum salt graphene and carbon nanotubes with an aluminum salt concentration of 4 mg / ml is dispersed by ultrasonic wave for 4 hours to obtain a mixed electrophoretic solution of uniformly dispersed aluminum salt graphene and carbon nanotubes;
[0041] (2) Ultrasonicate an aluminum sheet with a thickness of 0.1 mm in absolute ethanol solution for 10 minutes, then soak it in 6% dilute nitric acid for 1 minute, rinse it with deionized water several times, and use it as the cathode after drying;
[0042] (3) With the graphite sheet equiva...
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