Water-cured temperature-sensitive injection type dental root canal repair material and application thereof
A restorative material, injection-type technology, applied in dentistry, dental preparations, dental prosthesis, etc., can solve the problems affecting the treatment effect and success rate, low work efficiency, difficult operation, etc., to achieve good apical sealing and convenient operation , not easy to lose the effect
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Embodiment 1
[0048] Weigh 4.5 grams of tricalcium silicate / dicalcium silicate with particle size less than 10um, 0.3 grams of calcium hydroxide, 0.4 grams of tetracalcium phosphate, 0.4 grams of calcium hydrogen phosphate, 0.4 grams of hydroxyapatite, hydroxybutyl chitosan 0.5 grams, 1.5 grams of zirconium dioxide to form a mixture, and use 2 grams of glycerol to adjust it into a paste to obtain a root canal restoration material. The material is milky white, glossy, and has good fluidity, no layering, no phase separation, and a resting time of up to 183 days. See the appearance picture figure 1 , the effect of the material after curing is shown in figure 2 , figure 2 It can be seen that the material is still white and solid after curing, which will not cause tooth discoloration. Figure 5 It is the appearance of the aqueous solution of 5% hydroxybutyl chitosan. It can be seen from the figure that hydroxybutyl chitosan is still in solution at 25°C and has good fluidity, and it turns in...
Embodiment 2
[0051] Weigh 3.7 grams of tricalcium silicate / dicalcium silicate with particle size less than 10um, 0.5 grams of calcium hydroxide, 0.3 grams of tetracalcium phosphate, 0.5 grams of calcium hydrogen phosphate, 0.4 grams of hydroxyapatite, hydroxybutyl chitosan 0.8 grams, 0.5 grams of tantalum pentoxide, and 0.5 grams of zirconium dioxide are used to form a mixture, which is adjusted into a paste with 2.8 grams of water-soluble silicone oil and poured into a syringe. The material is milky white, lustrous, has good fluidity, and does not layer or phase separate.
Embodiment 3
[0053] Weigh 3.3 grams of tricalcium silicate / dicalcium silicate with particle size less than 10um, 0.2 grams of calcium hydroxide, 0.8 grams of tetracalcium phosphate, 0.7 grams of calcium hydrogen phosphate, 0.7 grams of hydroxyapatite, hydroxybutyl chitosan 1.0 g, 0.8 g of zirconium dioxide, and 0.5 g of barium sulfate form a mixture, which is adjusted into a paste with 2.0 g of polyethylene glycol, and poured into a syringe. The material is milky white, lustrous, has good fluidity, and does not layer or phase separate.
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