Sm-Gd-Dy tri-rare-earth ion tantalate and preparation method and application thereof
A technology of rare earth ions and tantalate, applied in the field of tantalate, can solve the problems of low temperature, coating failure, high melting point, etc., and achieve the effect of small grain size, less defects such as cracks, and high density
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[0027] The present invention will be further described in detail below with reference to the drawings and specific embodiments 1-8.
[0028] The Sm-Gd-Dy three rare earth ion tantalate provided by the present invention has the general chemical formula of Sm a Gd b Dy c TaO 7 , Where a+b+c=3, and a, b, c=0.8 to 1.2. In each embodiment, the coefficients of Sm, Gd, and Dy are shown in Table 1.
[0029] The preparation steps of the above Sm-Gd-Dy three rare earth ion tantalate are as follows:
[0030] (1) Weigh samarium nitrate (Sm(NO 3 ) 3 ), Gadolinium Nitrate (Gd(NO 3 ) 3 ), Dy(NO 3 ) 3 ) And tantalum oxalate (Ta 2 (C 2 O 4 ) 5 ), added to citric acid (C 6 H 8 O 7 In ), the specific addition amount of each embodiment is shown in Table 1 (it needs to be converted into mass when weighing, and in the present invention, it is measured by mole for the convenience of expressing the stoichiometric ratio). Incubate at 135°C for 50 minutes and perform vigorous mechanical stirring to make it f...
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