Spinning material capable of being quickly dissolved or dispersed and preparation method and application thereof
A spinning material and fast technology, applied in the direction of electrospinning, textiles and papermaking, single-component protein rayon, etc., can solve the problems of low solubility, slow evaporation rate, and reduce material porosity, etc., to achieve rich surface structure, Effects that are convenient to store and use
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Embodiment 1
[0020] Solvent preparation: Mix 500 parts by weight of deionized water and 500 parts of ethanol evenly, slowly add lactic acid dropwise until the pH value shows 4, slowly add glycerin, the amount of glycerin added is 5% of lactic acid, and stir evenly to obtain a colorless and transparent Electrospinning solvent; the dehydrated ethanol is wt99.5%, the food-grade citric acid is wt54%, the food-grade lactic acid is wt88%, and the food-grade glycerin is wt99.7%.
[0021] Configure the electrospinning stock solution: pour 1000 parts by weight of solvent and 250 parts by weight of pure collagen powder into a round bottom flask, and stir at 60°C to dissolve all the collagen into a colorless and transparent solution;
[0022] A small electrospinning equipment is selected: the receiving distance is 70mm; the diameter of the spinneret is 1.0mm; the electric field strength is 300kV / m; the drum receiver with a diameter of 150mm is used, and the rotation speed is 3600rpm; A spinning mater...
Embodiment 2
[0024] Solvent preparation: mix 700 parts by weight of deionized water and 300 parts of ethanol evenly, slowly add citric acid dropwise until the pH value shows 3, add glycerin dropwise, the amount of glycerol is 5% of citric acid, stir evenly to obtain a colorless Transparent electrospinning solvent; the dehydrated alcohol is wt99.5%, the food-grade citric acid is wt54%, the food-grade lactic acid is wt88%, and the food-grade glycerin is wt99.7% %.
[0025] Prepare electrospinning stock solution: pour 1000 parts by weight of solvent, 250 parts by weight of pure collagen powder, 100 parts by weight of chitosan, and 7 parts by weight of Yunnan Baiyao into a round bottom flask. Stir at 60°C to dissolve all the solid powder to obtain a colorless and transparent solution;
[0026] A small electrospinning equipment is selected: the receiving distance is 70mm; the diameter of the spinneret is 1.0mm; the electric field strength is 300kV / m; the drum receiver with a diameter of 150mm ...
Embodiment 3
[0028] Solvent preparation: mix 500 parts by weight of deionized water and 500 parts of ethanol evenly, slowly add lactic acid dropwise until the pH value shows 4, add glycerin dropwise, the amount of glycerin added is 5% of citric acid, and electromagnetically stir evenly to obtain a colorless Transparent electrospinning solvent; the dehydrated alcohol is wt99.5%, the food-grade citric acid is wt54%, the food-grade lactic acid is wt88%, and the food-grade glycerin is wt99.7% %.
[0029] Configure the electrospinning stock solution: pour 1000 parts by weight of solvent into the round bottom flask, 350 parts by weight of A collagen paste powder, stir at 60°C to completely dissolve the A collagen paste powder, and then filter it with an 80-mesh filter screen to obtain Reddish brown translucent electrospinning stock solution;
[0030] A small electrospinning equipment is selected: the receiving distance is 90mm; the diameter of the spinneret is 1.5mm; the electric field strength...
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