A reflective thermal insulation coating
A technology of reflective thermal insulation coating and silicophosphoric acid, which is used in reflective/signal coatings, anti-corrosion coatings, antifouling/underwater coatings, etc., can solve the problems of insufficient comprehensive performance of coatings, poor storage stability, and single film-forming substances. To achieve the effect of being conducive to heat insulation, fast curing speed, and low equipment requirements
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Embodiment 1
[0028] A reflective heat-insulating coating, comprising the following components in parts by mass: 50 parts of organosilicon phosphate film-forming ionic polymers, 7 parts of mesoporous silica, 7 parts of alumina nanotubes, 10 parts of water, wetting 1 part of dispersant polyacrylate, 1 part of defoamer polysiloxane, 1 part of glycerin.
[0029] The preparation method of described organosilicon phosphate ester film-forming ionic polymer, comprises the steps:
[0030] 1) Preparation of vinylimidazole salt: Dissolve 10g of vinylimidazole and 15g of 2-methoxyethoxymethyl chloride in 100g of ether, stir and react at room temperature for 4 hours, wash the product with ether for 4 times, and in The solvent was removed by rotary evaporation at room temperature;
[0031] 2) Preparation of film-forming polymer: 10 g of vinyl imidazolium salt, 10 g of bistrimethylsilylated vinyl phosphate, 10 g of vinyl ferrocene, 2,2,2-tris Dissolve 30g of fluoroethyl methacrylate and 0.3g of azobisi...
Embodiment 2
[0034] A reflective heat-insulating coating, comprising the following components in parts by mass: 53 parts of organosilicon phosphate film-forming ionic polymers, 9 parts of mesoporous silica, 9 parts of alumina nanotubes, 12 parts of ethanol, Wet dispersant sodium polyacrylate 1 part, defoamer polysiloxane 1 part, fluorine-modified acrylic leveling agent 1.5 parts, anti-ultraviolet additive UV-360 0.5 parts.
[0035] The preparation method of described organosilicon phosphate ester film-forming ionic polymer, comprises the steps:
[0036] 1) Preparation of vinylimidazole salt: Dissolve 10g of vinylimidazole and 17g of 2-methoxyethoxymethyl chloride in ether 130, stir and react at room temperature for 5 hours, wash the product 5 times with ether, And the solvent was removed by rotary evaporation at room temperature;
[0037] 2) Preparation of film-forming polymer: 13g of vinyl imidazolium salt, 10g of bistrimethylsilylated vinyl phosphate, 10g of vinyl ferrocene, 2,2,2-tris ...
Embodiment 3
[0040] A reflective heat-insulating coating, comprising the following components in parts by mass: 56 parts of organosilicon phosphate film-forming ionomers, 10 parts of mesoporous silica, 10 parts of alumina nanotubes, 13 parts of isopropanol, 2 parts of anti-settling agent polyethylene wax, 1 part of anti-ultraviolet additive, 1 part of defoamer Deqian 3100, 1 part of antifreeze agent sodium nitrite.
[0041] The preparation method of described organosilicon phosphate ester film-forming ionic polymer, comprises the steps:
[0042] 1) Preparation of vinylimidazole salt: Dissolve 10g of vinylimidazole and 18g of 2-methoxyethoxymethyl chloride in 140g of ether, stir and react at room temperature for 5.5 hours, wash the product with ether for 6 times, and in The solvent was removed by rotary evaporation at room temperature;
[0043] 2) Preparation of film-forming polymer: 17g of vinylimidazolium salt, 10g of bistrimethylsilylated vinyl phosphate, 10g of vinyl ferrocene, 2,2,2-tri...
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