Graphene heating film suitable for power cell bag and graphite alkene heating film assembly
A technology of ene heating film and graphene, which is applied in the direction of heating element materials, ohmic resistance heating, electrical components, etc., can solve the problems of heat resistance, wear resistance, moisture resistance and safety, the heating circuit does not have good flexibility, Large radiation heat loss and other problems, to achieve the effect of soft texture, fast heating speed, high electric heating efficiency
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[0040] (II) the preparation method of this graphene conductive paste
[0041] The preparation method of this graphene conductive paste comprises the following steps:
[0042] Epoxy functionalization of graphene powder: epoxy functionalization of graphene powder with epoxy resin, wherein the weight ratio of the epoxy resin to the graphene powder is 1:4-3:1;
[0043] Epoxy modification of siloxane: modify siloxane with epoxy resin, wherein the weight ratio of the epoxy resin to the siloxane is 1:3-2:1;
[0044] Mixing: 1-10 parts by weight of the surface-functionalized graphene powder, 2-6 parts by weight of the epoxy-modified siloxane, 4-15 parts by weight of the epoxy resin, and epoxy reactive diluent 2-6 parts by weight and 0.1-0.8 parts by weight of latent curing agent are subjected to low-speed dispersion stirring, high-speed dispersion stirring, and vacuum defoaming to prepare the graphene conductive paste.
[0045] Preferably, the epoxy resin is an epoxy resin with a π ...
preparation example 1
[0055] In this preparation example, the epoxy resin for epoxy functionalization of graphene, the epoxy resin for epoxy modification of siloxane and the epoxy resin as one of the main components of graphene conductive paste are all used Bisphenol A type epoxy resin. The bisphenol A epoxy resin was purchased from Shenzhen Jiadida Chemical Co., Ltd., and the model was NPEL-128E.
[0056] Add 2g of graphene powder (highly conductive graphene powder prepared by Shenzhen Shiwang New Material Technology Co., Ltd.), 3.5g of bisphenol A epoxy resin and 200g of absolute ethanol into the medium and high-speed rotating chamber testing machine middle. The high-speed rotating cavity testing machine is equipped with an ultrasonic generator and a heating constant temperature device. The mixture is rotated at 20-120°C, 1600rpm at high speed and 2000W, frequency 80KHz ultrasonic waves are shaken for 1-8h for 1-8 hours, then vacuum filtered and dried at a temperature lower than 50°C, and the s...
preparation example 2
[0060] In this preparation example, the epoxy resin for epoxy functionalization of graphene, the epoxy resin for epoxy modification of siloxane and the epoxy resin as one of the main components of graphene conductive paste are all used Bisphenol F type epoxy resin replaces the bisphenol A type epoxy resin in Preparation Example 1, and the rest are the same as Preparation Example 1. The bisphenol F epoxy resin was purchased from Shenzhen Jiadida Chemical Co., Ltd., and the model was NPEF-170. Preparation example 3
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