A kind of preparation method of glass fiber sizing agent
The technology of glass fiber and sizing agent is applied in the field of preparation of glass fiber sizing agent, which can solve the problems of reducing the economic benefit of glass fiber, sticking filaments of spools, and easily damaged fibers, etc., and achieves uniform adsorption surface and lower surface energy. , the effect of easy adsorption
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Embodiment 1
[0020] A preparation method of glass fiber sizing, the specific steps are as follows:
[0021] Step 1, configure the hydrolysis solution: Stir the glacial acetic acid and soft water evenly to obtain the hydrolysis solution. The mass ratio of glacial acetic acid and soft water is 1.6:997;
[0022] Step 2, configure the dispersion: add r-methacryloxypropyltrimethoxysilane to the hydrolysis solution and ultrasonically oscillate evenly, the quality of r-methacryloxypropyltrimethoxysilane and hydrolysis solution The ratio is 2.3:995, obtains dispersion liquid;
[0023] Step 3, configure the lubricant liquid: mix soft water, disodium ethoxylated alcohol sulfosuccinate, polyethylene glycol and cationic film according to the mass ratio of 86:2.6:3.8:6.6 and stir evenly at a speed of 120rpm to obtain a lubricant liquid;
[0024] Step 4, configure the mixed solution: add the binder, lubricant liquid, antistatic agent and epoxy emulsion to the dispersion in turn and stir for 36 minutes...
Embodiment 2
[0027] A preparation method of glass fiber sizing, the specific steps are as follows:
[0028] Step 1, configure the hydrolysis solution: Stir the glacial acetic acid and soft water evenly to obtain the hydrolysis solution, the mass ratio of glacial acetic acid and soft water is 1:499;
[0029] Step 2, configure the dispersion: add the coupling agent to the hydrolysis solution and oscillate uniformly, the power of the ultrasonic oscillation is 175W, the frequency of the ultrasonic oscillation is 38KHz, the mass ratio of the coupling agent to the hydrolysis solution is 3:997, and the obtained Dispersions;
[0030] Step 3, configure the lubricant liquid: mix soft water, disodium ethoxylated alcohol sulfosuccinate, polyethylene glycol and cationic film according to the mass ratio of 89:3:4:7 and stir evenly at a speed of 135rpm to obtain a lubricant liquid;
[0031] Step 4, configure the mixed solution: add vinyl acetate-acrylate, lubricant liquid, lithium chloride and bispheno...
Embodiment 3
[0038] A preparation method of glass fiber sizing, the specific steps are as follows:
[0039] Step 1, configure the hydrolysis solution: Stir the glacial acetic acid and soft water evenly to obtain the hydrolysis solution. The mass ratio of glacial acetic acid and soft water is 3:999;
[0040] Step 2, configure the dispersion: add r-methacryloxypropyltrimethoxysilane to the hydrolysis solution and oscillate evenly with ultrasonic waves. The power of ultrasonic oscillations is 190W, and the frequency of ultrasonic oscillations is 36-40KHz. The mass ratio of acryloyloxypropyltrimethoxysilane and the hydrolysis solution is 4.5:998 to obtain a dispersion;
[0041] Step 3, configure the lubricant liquid: mix soft water, disodium ethoxylated alcohol sulfosuccinate, polyethylene glycol and cationic film according to the mass ratio of 91:3.5:4.4:7.5 and stir at a speed of 90rpm to obtain a lubricant liquid;
[0042] Step 4, configure the mixed solution: add vinyl acetate-acrylate, ...
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