Traditional Chinese medicine preservation agent with oxygen slow-release function as well as preparation method and use method of traditional Chinese medicine preservation agent
A technology of traditional Chinese medicinal materials and curing agents, applied in chemical instruments and methods, chemical/physical/physical chemical processes, chemical/physical processes, etc., can solve problems such as poor effects, prevent low oxygen content, improve quality, and reduce sulfur The effect of content
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Embodiment 1
[0055] Zeolite is selected as the porous carrier.
[0056] The first step, pretreatment of porous minerals
[0057] The porous zeolite is crushed and passed through a 100-mesh sieve, soaked in a hydrochloric acid solution with a concentration of 8wt% for 12 hours, neutralized by adding sodium carbonate to a pH value of about 7, filtered, calcined in a muffle furnace at 400°C for 3 hours, and cooled for later use ;
[0058] The second step is to load calcium peroxide oxygen slow-release agent on the surface of the porous material
[0059] At room temperature, under the condition of stirring, add zeolite powder in water, the mass ratio of water and powder is 5:1, add 294 grams of CaCl per kilogram of water and porous powder mixed liquid 2 2H 2 O and H at a concentration of 30% by volume 2 o 2 205ml, add concentrated NH dropwise while stirring 3 ·H 2 O solution, adjust the pH value in the range of 11.0-12.0. After reacting for 20 minutes, add ice cubes to cool, filter and ...
Embodiment 2
[0067] Activated carbon powder is selected as the porous carrier.
[0068] In the first step, activated carbon powder purchased from the market does not require acid pretreatment.
[0069] The second step is to load calcium peroxide oxygen slow-release agent on the surface of the porous material
[0070] At room temperature, under the condition of stirring, add activated carbon powder in water, the mass ratio of water and powder is 6:1, add 294 grams of CaCl to the mixed liquid of per kilogram of water and porous powder 2 2H 2 O and H at a concentration of 30% by volume 2 o 2 205ml, add concentrated NH dropwise while stirring 3 ·H 2 O solution, adjust the pH value in the range of 11.0-12.0, react for 20 minutes, add ice cubes to cool, filter with suction and place in a constant temperature box, first bake at 60°C for 0.5 hours, then at 140°C for 0.5 hours, turn to After cooling in a desiccator, it is vacuum-packed and placed in a desiccant that absorbs moisture. Place i...
Embodiment 3
[0078] Attapulgite clay mineral is selected as the porous mineral carrier.
[0079] The first step, pretreatment of porous minerals
[0080] After crushing the porous attapulgite clay, pass it through a 100-mesh sieve, soak it in a hydrochloric acid solution with a concentration of 6wt% for 24 hours, add sodium carbonate to neutralize it to a pH value of about 7, filter it, and calcinate it in a muffle furnace at 500°C for 2 hours, then cool it Backup.
[0081] The second step is to load calcium peroxide oxygen slow-release agent on the surface of the porous material
[0082] At room temperature, under the condition of stirring, add porous material powder in water, the mass ratio of water and powder is 3:1, add 294 grams of CaCl per kilogram of water and porous powder mixed liquid 2 2H 2 O and H at a concentration of 30% by volume 2 o 2 205ml, add concentrated NH dropwise while stirring 3 ·H 2 O solution, adjust the pH value in the range of 11.0-12.0. After reacting for...
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