Adhesive composition and surface protection film
A composition and adhesive technology, applied in the directions of adhesives, adhesive types, ester copolymer adhesives, etc., can solve the problems of floating, poor re-peelability, etc., and achieve excellent adhesion performance, high utilization value, and excellent resistance. The effect of stripping electrostatic properties
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Embodiment 1
[0103] Nitrogen gas was introduced into a reaction device having a stirrer, a thermometer, a reflux cooler, and a nitrogen gas introduction pipe, and the air in the reaction device was replaced with nitrogen gas. Then, add 90 parts by weight of 2-ethylhexyl acrylate, 10 parts by weight of methyl acrylate, 5.5 parts by weight of 8-hydroxyoctyl acrylate, 0.2 parts by weight of acrylic acid, while adding solvent (ethyl acetate). Then, 0.1 weight part of azobisisobutyronitrile was dripped as a polymerization initiator over 2 hours, and it was made to react at 65 degreeC for 6 hours, and the acrylic polymer solution used in Example 1 was obtained.
Embodiment 2~6 and comparative example 1~3
[0105] Examples 2 to 6 were obtained in the same manner as the acrylic polymer solution used in Example 1 above, except that the compositions of the monomers were as described in (A) to (C) of Table 1, respectively. And the acrylic polymer solution used in Comparative Examples 1-3.
[0106]
[0107] [Example 1]
[0108] To the acrylic polymer solution of Example 1 prepared as described above, 2.0 parts by weight of a crosslinking agent (CORONATE HX), 9 parts by weight of a crosslinking retarder (acetylacetone), and 0.1 parts by weight of a crosslinking agent (CORONATE HX) were added. Catalyst (titanium triacetylacetonate), 0.9 parts by weight of antistatic agent (methyl trioctyl ammonium tris (pentafluorobenzenesulfonyl) methide salt), 0.05 parts by weight of polyether modified siloxane compound (HLB =7) and 0.2 parts by weight of copolymer B-1 (molecular weight: 150,000) were stirred and mixed to obtain the adhesive composition of Example 1. After applying this adhesive c...
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