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Glass fibre reinforced plastic septic-tank glue and preparation method thereof

A glass tempering and septic tank technology, applied in the field of glass fiber reinforced plastics, can solve problems such as poor temperature resistance, odor generation, human health hazards, etc. Effect

Inactive Publication Date: 2019-01-25
安徽汇创新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In the prior art, although the septic tank made of fiberglass has superior performance, its temperature resistance is still poor, and it will produce odor during the heating process, which is harmful to human health.

Method used

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  • Glass fibre reinforced plastic septic-tank glue and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A kind of fiberglass septic tank compound, its raw material comprises by weight: 20 parts of unsaturated polyester resin, 20 parts of epoxy-modified phenolic resin, 8 parts of glass fiber, 15 parts of flame retardant, 6 parts of silicon carbide micropowder, 10 parts of quartz powder, 1 part of calcium stearate, 10 parts of titanate coupling agent, 0.1 part of antioxidant, 0.3 part of lubricant;

[0022] Wherein, the unsaturated polyester resin is prepared by the following process: 17 parts by weight of maleic anhydride, 28 parts of tetrahydrophthalic anhydride, 4 parts of adipic acid, 38 parts of propylene glycol, 4 parts of diethylene glycol After mixing the parts, raise the temperature to 160°C and stir the reaction for 0.5h, continue to raise the temperature to 220°C, stir the reaction until the acid value is lower than 15mgKOH / g, cool down to 90°C, pass nitrogen, and then add N-(polydimethylsilane Mix 12 parts of oxane)maleimide and 0.1 part of dibenzoyl peroxide, h...

Embodiment 2

[0026] A kind of fiberglass septic tank compound, its raw material comprises by weight: 40 parts of unsaturated polyester resin, 10 parts of epoxy modified phenolic resin, 15 parts of glass fiber, 5 parts of flame retardant, 18 parts of silicon carbide micropowder, 4 parts of quartz powder, 5 parts of calcium stearate, 3 parts of titanate coupling agent, 0.5 part of antioxidant, 0.1 part of lubricant;

[0027]Wherein, the unsaturated polyester resin is prepared by the following process: 28 parts by weight of maleic anhydride, 12 parts of tetrahydrophthalic anhydride, 12 parts of adipic acid, 23 parts of propylene glycol, 8 parts of diethylene glycol After mixing the parts, heat up to 140°C and stir for 1 hour, continue to heat up to 200°C, stir and react until the acid value is lower than 15mgKOH / g, cool down to 100°C, pass nitrogen, and then add N-(polydimethylsiloxane Mix 5 parts of alk)maleimide and 0.5 part of dibenzoyl peroxide, heat up to 120°C, stir and react for 1 h, a...

Embodiment 3

[0031] A kind of fiberglass septic tank compound, its raw material comprises by weight: 30 parts of unsaturated polyester resins, 15 parts of epoxy-modified phenolic resins, 12 parts of glass fibers, 10 parts of flame retardants, 12 parts of silicon carbide micropowders, 7 parts of quartz powder, 3 parts of calcium stearate, 6 parts of titanate coupling agent, 0.3 part of antioxidant, 0.2 part of lubricant;

[0032] Wherein, the unsaturated polyester resin is prepared by the following process: 23 parts by weight of maleic anhydride, 20 parts of tetrahydrophthalic anhydride, 8 parts of adipic acid, 30 parts of propylene glycol, 6 parts of diethylene glycol After mixing the parts, raise the temperature to 145°C, stir and react for 0.8h, continue to raise the temperature to 205°C, stir and react until the acid value is lower than 15mgKOH / g, cool down to 95°C, pass nitrogen, and then add N-(polydimethylsilane Mix 8 parts of oxane)maleimide and 0.3 parts of dibenzoyl peroxide, heat...

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Abstract

The invention discloses glass fibre reinforced plastic septic-tank glue. The glass fibre reinforced plastic septic-tank glue is prepared from the following raw materials in parts by weight: 20-40 parts of unsaturated polyester resin, 10-20 parts of epoxy modified phenolic resin, 8-15 parts of glass fibres, 5-15 parts of a flame retardant, 6-18 parts of silicon carbide micro powder, 4-10 parts of quartz powder, 1-5 parts of calcium stearate, 3-10 parts of a titanate coupling agent, 0.1-0.5 part of an anti-oxidant, and 0.1-0.3 part of a lubricant; and the unsaturated polyester resin is preparedby the following process comprising the following steps: mixing maleic anhydride, tetrahydrophthalic anhydride, adipic acid, propylene glycol and diethylene glycol, heating up and performing stirringreaction, adding N-(polydimethylsiloxane) maleimide and dibenzoyl peroxide to heat and perform stirring reaction; and adding hydroquinone and styrene to uniformly mix to obtain high-temperature-resistant unsaturated polyester resin. The glass fibre reinforced plastic septic-tank glue has good high temperature resistance and good mechanical property, is good in processability, is low in toxicity and is environmentally friendly.

Description

technical field [0001] The invention relates to the technical field of glass fiber reinforced plastics, in particular to a rubber material for glass fiber reinforced plastic septic tanks and a preparation method thereof. Background technique [0002] Septic tank is an indispensable drainage treatment equipment in the construction field. It is used to discharge domestic wastewater into municipal pipelines after primary treatment or into lower-level sewage treatment facilities for advanced treatment. Most of them are buried. In the early days, septic tanks were usually made of bricks, reinforced concrete or steel plates, but they all had obvious defects. In recent years, glass fiber reinforced plastic septic tanks have gradually been selected by most construction units. The scientific name of FRP is glass fiber reinforced plastic, and the septic tank storage tank made of FRP has the characteristics of strong corrosion resistance, no leakage, easy construction, and slow aging s...

Claims

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Application Information

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IPC IPC(8): C08L67/06C08L61/14C08L83/04C08K13/04C08K7/14C08K3/34C08K3/36C08K5/098C08K5/10C08K3/22C08K5/092C08K7/26C08K3/38C08K5/41C08K5/134C08K5/526
CPCC08K2003/387C08L67/06C08L2201/08C08L61/14C08L83/04C08K13/04C08K7/14C08K3/34C08K3/36C08K5/098C08K5/10C08K3/2279C08K5/092C08K7/26C08K3/38C08K5/41C08K5/1345C08K5/526
Inventor 周飞任旭明汤明明
Owner 安徽汇创新材料有限公司
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