Azo pigment, colorant for color filter, coloring composition for color filter, and color filter
A color filter and coloring composition technology, applied in the field of color filters, can solve the problems of insufficient brightness, poor spectral shape, and low spectral transmittance, and achieve good storage stability and fastness Excellent, low stain migration effect
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Embodiment 1
[0315] (Manufacture of Azo Pigment 1)
[0316]
[0317] After adding 185 parts of base compound [B-1] to 1500 parts of N-methylpyrrolidone, 294 parts of 35% hydrochloric acid were added, and it cooled to -2-0 degreeC. After adding 208 parts of 25% sodium nitrite aqueous solution to this solution, it stirred for 30 minutes, maintaining at 0-5 degreeC, and prepared the diazonium solution. Separately, a coupling agent solution composed of 167 parts of coupling agent compound [C-1], 316 parts of 25% sodium hydroxide solution, and 1500 parts of methanol was prepared. The prepared diazonium solution and coupling agent solution were dropped into 1000 parts of acetic acid buffer solution of pH 5.4 at the same time for 10 minutes. After the dropwise addition was completed, after stirring at room temperature for 30 minutes, further, while maintaining stirring at 80° C., the precipitated reactant was filtered off, washed with hot water, and dried to obtain 343 parts of azo pigment 1 ...
Embodiment 2
[0321] (Manufacture of Azo Pigment 2)
[0322] In place of 185 parts of the basic compound [B-1] used in the production of the azo pigment 1, 169 parts of the basic compound [B-2] were used, and the same operation as the production of the azo pigment 1 was performed. , 337 parts of Azo Pigment 2 were obtained (yield: 98.1%). Based on the results of TOF-MS mass spectrometry and elemental analysis, it was identified as azo pigment 2.
[0323] Azo Pigment 2
[0324]
Embodiment 3
[0326] (Manufacture of Azo Pigment 3)
[0327] In place of 185 parts of the basic compound [B-1] used in the production of the azo pigment 1, 210 parts of the basic compound [B-3] were used, and the same operation as the production of the azo pigment 1 was performed. , 371 parts of Azo Pigment 3 were obtained (yield: 96.7%). Based on the results of TOF-MS mass spectrometry and elemental analysis, it was identified as azo pigment 3.
[0328] Azo Pigment 3
[0329]
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