Preparation method of aerogel composite thermal insulation material
A technology of composite thermal insulation material and aerogel, which is applied in the field of thermal insulation materials, can solve the problems of large amount of by-product hydrochloric acid, prolonged preparation cycle, corrosion of production equipment, etc., and achieve low production cost, reduced production cost, and small equipment loss.
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[0022] The invention provides a method for preparing an airgel composite thermal insulation material, comprising the following steps:
[0023] a) mixing a silicon source, hexamethyldisilazane, a pH regulator and a solvent to obtain a silica sol precursor solution;
[0024] b) impregnating the silica sol precursor solution into a magnesium silicate fiber mat and leaving it to stand to form a wet gel mat;
[0025] c) Soaking the wet gel felt into organosiloxane at 40-90° C., taking it out and drying it with microwave heating to obtain an airgel composite thermal insulation material.
[0026] In the method provided by the present invention, the silicon source, hexamethyldisilazane, pH regulator and solvent are firstly mixed. Wherein, the silicon source includes but not limited to one or more of sodium silicate, acidic silica sol, alkaline silica sol, methyl orthosilicate and ethyl orthosilicate; agent and / or alkaline pH adjuster, said acidic pH adjuster includes but not limited...
Embodiment 1
[0032] (1) Preparation of silica sol precursor:
[0033] Prepare 8wt% industrial water glass solution and 20wt% nitric acid solution with deionized water at 5°C; first inject 10mL of absolute ethanol at 5°C into the stirrer, start stirring, and then add 6mL of hexamethyldisilazide in sequence Alkanes, 20mL of the nitric acid solution, and continued to stir for 10min; then add 40mL of the industrial water glass solution to it, and control the pH of the silica sol precursor solution to 5.4.
[0034] (2) Choose a bulk density of 96kg / m 3 Magnesium silicate fiber needle-punched felt (fiber diameter 2-5 μm) is used as the base material, and it is laid flat in a closed container around it, and the above-mentioned silica sol precursor solution is poured into the container to make the magnesium silicate fiber needle-punched The felt is saturated to adsorb the silica sol precursor solution.
[0035] (3) Let the needle-punched felt treated in step (2) stand for 10 minutes to form a we...
Embodiment 2
[0040] (1) Preparation of silica sol precursor:
[0041] Prepare 8wt% industrial water glass solution and 20wt% nitric acid solution with deionized water at 5°C; first inject 10mL of absolute ethanol at 5°C into the stirrer, start stirring, and then add 6mL of hexamethyldisilazide in sequence Alkanes, 20mL of the nitric acid solution, and continued to stir for 10min; then add 40mL of the industrial water glass solution to it, and control the pH of the silica sol precursor solution to 5.4.
[0042] (2) Choose a bulk density of 128kg / m 3 Magnesium silicate fiber needle-punched felt (fiber diameter 2-5 μm) is used as the base material, and it is laid flat in a closed container around it, and the above-mentioned silica sol precursor solution is poured into the container to make the magnesium silicate fiber needle-punched The felt is saturated to adsorb the silica sol precursor solution.
[0043] (3) Let the needle-punched felt treated in step (2) stand for 10 minutes to form a w...
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