Porous nano-material and preparation method thereof
A technology of nanomaterials and raw materials, applied in the field of porous nanomaterials and their preparation, can solve the problems of poor adsorption capacity, re-desorption and release when the temperature rises or the concentration of pollutants drops, slow purification speed, and furniture damage, etc. The effect of decomposing, eliminating odor and improving efficiency
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Embodiment 1
[0041] A porous nanomaterial is prepared from the following raw materials by weight: 10 parts of azo compounds, 20 parts of secondary polyamide-amine dendrimer, 30 parts of nano-titanium dioxide, 5 parts of pyridyl porphyrin and deionized 80 parts of water.
[0042] The structural formula of azo compounds is:
[0043]
[0044] where R 1 , R 2 , R 3 and R 4 are alkyl, ester, hydroxyl and carboxyl groups, respectively, R 5 is an ester group.
[0045] The structural formula of the second-generation polyamide-amine dendrimer is:
[0046]
[0047] A preparation method of a porous nanomaterial, the preparation method comprising the following steps:
[0048] (1) respectively take by weighing 10 parts of azo compounds, 20 parts of secondary polyamide-amine dendrimer, 30 parts of nano titanium dioxide, 5 parts of pyridyl porphyrin and 80 parts of deionized water;
[0049] (2) deionized water, azo compounds and secondary polyamide-amine dendrimer taken in step (1) are put ...
Embodiment 2
[0053] A porous nanomaterial prepared from the following raw materials by weight: 12 parts of azo compounds, 25 parts of third-generation polyamide-amine dendrimer, 35 parts of nano-zinc oxide, 6 parts of methylene blue and deionized water 85 servings.
[0054] The structural formula of azo compounds is:
[0055]
[0056] where R 1 , R 2 , R 3 and R 4 are ester group, hydroxyl group, carboxyl group and amino group, respectively, R 5 is hydroxyl.
[0057] The structural formula of the third-generation polyamide-amine dendrimer is:
[0058]
[0059] A preparation method of a porous nanomaterial, the preparation method comprising the following steps:
[0060] (1) respectively take by weighing 12 parts of azo compounds, 25 parts of third-generation polyamide-amine dendrimer, 35 parts of nano-zinc oxide, 6 parts of methylene blue and 85 parts of deionized water;
[0061] (2) deionized water, azo compounds and three-generation polyamide-amine dendrimer taken by weighin...
Embodiment 3
[0065] A porous nanomaterial, prepared from the following raw materials by weight: 15 parts of azo compounds, 30 parts of secondary polyamide-amine dendrimer, 40 parts of nano silver, 7 parts of hematoporphyrin and deionized water 90 servings.
[0066] The structural formula of azo compounds is:
[0067]
[0068] where R 1 , R 2 , R 3 and R 4 are hydroxyl, carboxyl, amino and ester groups, respectively, R 5 is a carboxyl group.
[0069] The structural formula of the second-generation polyamide-amine dendrimer is:
[0070]
[0071] A preparation method of a porous nanomaterial, the preparation method comprising the following steps:
[0072] (1) respectively take by weighing 15 parts of azo compounds, 30 parts of secondary polyamide-amine dendrimer, 40 parts of nano silver, 7 parts of hematoporphyrin and 90 parts of deionized water;
[0073] (2) deionized water, azo compounds and secondary polyamide-amine dendrimer taken by weighing in step (1) are put into the hig...
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