Haze-reduction paint for building wall surfaces and preparation method
A coating and construction technology, applied in the field of haze-reducing coatings and preparations for building walls, can solve problems such as unsatisfactory haze removal effects, and achieve the effects of high specific surface area, strong adhesion, and high crystal phase purity
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Embodiment 1
[0031] (1) Mix zinc acetate dihydrate and diethylene glycol in proportion, add tourmaline nanoparticles with a particle size of 740nm and sonicate for 20 minutes, and the weight ratio of zinc acetate dihydrate, diethylene glycol, and tourmaline nanoparticles is 0.035:1 :5, after zinc acetate dihydrate is completely dissolved, continue to stir, heat to 160°C, age at a constant temperature for 1h, stop heating, centrifuge after natural cooling, and wash repeatedly with absolute ethanol to obtain tourmaline-loaded zinc oxide nanocrystals, oxidized The loading of zinc nanocrystals is 21%, and then dried in an oven at 80°C;
[0032] (2) In the solution concentration of 80g / L sodium bicarbonate solution, the drop rate is 0.25 mL·min -1 Slowly add a sodium metaaluminate solution with a solution concentration of 120g / L, fully stir at 25°C to react, collect the formed precipitate and wash it with deionized water to obtain an aluminum hydroxide filter cake; then mix the aluminum hydroxi...
Embodiment 2
[0036] (1) Mix zinc acetate dihydrate and diethylene glycol in proportion, add tourmaline nanoparticles with a particle size of 120nm and sonicate for 20 minutes, and the weight ratio of zinc acetate dihydrate, diethylene glycol, and tourmaline nanoparticles is 0.032:1 : 6. After zinc acetate dihydrate is completely dissolved, continue to stir, heat to 155° C., age at a constant temperature for 1 hour, stop heating, centrifuge after natural cooling, and repeatedly wash with absolute ethanol to obtain tourmaline-loaded zinc oxide nanocrystals, oxidized The loading of zinc nanocrystals is 23%, and then dried in an oven at 80°C;
[0037] (2) In the solution concentration of 60-100g / L sodium bicarbonate solution, the drop rate is 0.45mL·min -1 Slowly add a sodium metaaluminate solution with a solution concentration of 130g / L, fully stir the reaction at 25°C, collect the formed precipitate and wash it with deionized water to obtain an aluminum hydroxide filter cake; then add the al...
Embodiment 3
[0041] (1) Mix zinc acetate dihydrate and diethylene glycol in proportion, add tourmaline nanoparticles with a particle size of 500nm and sonicate for 20 minutes, and the weight ratio of zinc acetate dihydrate, diethylene glycol, and tourmaline nanoparticles is 0.01:1 :3. After the zinc acetate dihydrate is completely dissolved, continue to stir, heat to 156°C, age at a constant temperature for 1 hour, stop heating, centrifuge after natural cooling, and wash repeatedly with absolute ethanol to obtain tourmaline-loaded zinc oxide nanocrystals, oxidized The loading of zinc nanocrystals was 16%, and then dried in an oven at 80 °C;
[0042] (2) In the solution concentration of 60-100g / L sodium bicarbonate solution, the drop rate is 0.24mL·min -1 Slowly add a sodium metaaluminate solution with a solution concentration of 143g / L, fully stir at 25°C for the reaction, collect the formed precipitate and wash it with deionized water to obtain an aluminum hydroxide filter cake; then add ...
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