Co-modified Ni<2+> doped modified Ta3N5 photocatalytic hydrogen-producing material and preparation method thereof
A technology of hydrogen materials and photocatalysis, applied in the direction of physical/chemical process catalysts, hydrogen production, chemical instruments and methods, etc., can solve the problems of destroying the stability of material structures, achieve enhanced structural and chemical stability, and promote Separation and transport process, the effect of enhancing electron transport performance
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[0024] Co-modified Ni 2+ Doped modified Ta 3 N 5The preparation method of photocatalytic hydrogen production material comprises the following steps:
[0025] (1) Add an appropriate amount of absolute ethanol and distilled water as a mixed solvent into the reaction flask, the volume ratio of the two is 5-7:1, add 90-95 parts of TaCl 5 Stir until dissolved, slowly add NaOH while stirring to adjust the pH of the solution to 11-12, then add 3-6 parts of NiCl 2 , transfer the solution into an automatic hydrothermal reaction kettle, raise the temperature to 170-180°C, stir at a constant speed for 4-6 hours, cool the solution to room temperature, filter to remove the solvent, wash the solid product with distilled water, and place it in a blast dryer Heating to 80-90°C and fully drying to obtain a Ni-Ta precursor.
[0026] (2) Place the Ni-Ta precursor in an atmosphere resistance furnace, and feed air and high-purity O 2 , the volume ratio of the two is 10-15:1, the heating rate ...
Embodiment 1
[0031] (1) Preparation of Ni-Ta precursor 1: add an appropriate amount of absolute ethanol and distilled water as a mixed solvent into the reaction flask, the volume ratio of the two is 5:1, add 95 parts of TaCl 5 Stir until dissolved, slowly add NaOH while stirring to adjust the pH of the solution to 11, then add 3 parts of NiCl 2 , transfer the solution into an automatic hydrothermal reaction kettle, raise the temperature to 170°C, stir at a constant speed for 4 hours, cool the solution to room temperature, remove the solvent by filtration, wash the solid product with distilled water, and heat it to 80°C in a blast dryer Fully dried to obtain Ni-Ta precursor 1.
[0032] (2) Preparation of Ni 2+ Doping Ta 2 o 5 Compound 1: The Ni-Ta precursor 1 was placed in an atmosphere resistance furnace, and air and high-purity O 2 , the volume ratio of the two is 10:1, the heating rate of the atmosphere resistance furnace is 5 ℃ / min, rise to 750 ℃, heat preservation and calcination f...
Embodiment 2
[0037] (1) Preparation of Ni-Ta precursor 2: add an appropriate amount of absolute ethanol and distilled water as a mixed solvent into the reaction flask, the volume ratio of the two is 6:1, add 94 parts of TaCl 5 Stir until dissolved, slowly add NaOH while stirring to adjust the pH of the solution to 11, then add 3.5 parts of NiCl 2 , transfer the solution into an automatic hydrothermal reaction kettle, raise the temperature to 175°C, stir at a constant speed for 5 hours, cool the solution to room temperature, remove the solvent by filtration, wash the solid product with distilled water, and heat it to 85°C in a blast dryer Fully dried to obtain Ni-Ta precursor 2.
[0038] (2) Preparation of Ni 2+ Doping Ta 2 o 5 Compound 2: The Ni-Ta precursor 2 was placed in an atmosphere resistance furnace, and air and high-purity O 2 , the volume ratio of the two is 12:1, the heating rate of the atmosphere resistance furnace is 8°C / min, rise to 750°C, heat preservation and calcination...
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