Preparation method of magnesium-erbium-cerium fused fireproof profile

A profile and refractory technology, which is applied in the field of preparation of magnesium-erbium-cerium fused refractory profiles, can solve the problems of wasting energy, deformation and aliasing, surface layer formation, etc., and achieves the effects of saving mineral resources, good stretchability, and stable properties.

Inactive Publication Date: 2020-04-10
任有科
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Traditional process: need to go through raw material large crystallization, magnesium aluminum zirconium crystal stone, magnesium aluminum crystal stone for proportioning - adding binder mixture - pouring into the mold - extruding through a press - heating and drying (conditions of 200 degrees Celsius) -It is fired with light oil in the kiln, which has experienced two high temperatures, wasting energy, and the yield per ton is only 70%
[0004] The disadvantage is that it is afraid of moisture and water immersion. It is generally operated and transported to the user immediately after the finished product to avoid deformation of the product.

Method used

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  • Preparation method of magnesium-erbium-cerium fused fireproof profile

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] 925kg of magnesia, 30kg of erbium oxide, 15kg of zirconium oxide, 30kg of cerium oxide, all the raw materials are stirred evenly and mixed with water to form pellets with a diameter of 2cm. The melting temperature is between 3200℃-3600℃, and the microwave vibration mode is used in the melting process to melt all the materials in the furnace, so that there are no grade blocks and under-melting materials in the furnace. After all the raw materials in the furnace are melted, the electrodes are taken out, and the solution in the furnace is poured into a high-temperature profile mold, and after cooling, a finished block of 965kg is obtained.

Embodiment 2

[0032] 970kg of magnesia, 10kg of erbium oxide, 5kg of zirconium oxide, 15kg of cerium oxide, the production method is the same as that of Example 1, and 970kg of finished product block is obtained.

Embodiment 3

[0034] 950kg of magnesia, 20kg of erbium oxide, 10kg of zirconium oxide, 20kg of cerium oxide, the production method is the same as that of Example 1, and 965kg of finished product block is obtained.

[0035] The physical and chemical indicators of the product: the density is 4.2g / cm3, the compressive capacity is 520MPa, the refractoriness is 2850℃, the opening rate is 0%, the thermal shock stability is 1300℃, and the air cooling is more than 100 times.

[0036] The finished products produced by the process of the present application are directly usable profiles. The basic specifications of the current products are 900mm*900mm*900mm, 500mm*500mm*500mm, 400mm*400mm*400mm, and there are more than 300 kinds of functional originals.

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Abstract

The invention discloses a preparation method of a magnesium-erbium-cerium fused fireproof profile, and relates to the technical field of fused fireproof profiles. The preparation method comprises following steps: weighing following raw materials: magnesia, erbium oxide, zirconia, and cerium oxide, wherein in the raw materials, magnesium accounts for 92.5 to 97 parts, erbium accounts for 1 to 3 parts, zirconium accounts for 0.5 to 1.5 parts, and cerium accounts for 1.5 to 3 parts; mixing and evenly stirring the raw materials in a mixing device; adding water, stirring to form a mixed material; drying the mixed material, adding the mixed material into an arc furnace at a time, fusing the mixed material, wherein during the fusion process, a microwave vibration mode is adopted, after the mixedmaterial is completely melted, taking out the electrodes, pouring the solution in the furnace into a profile grinding tool, and cooling. Cerium oxide and erbium oxide are added to improve the toughness and slag erosion resistant performance of the profile; one-time smelting and moulding is adopted, during the fusion process, a microwave vibration mode is adopted, the porosity of the profile is reduced, and the output and quality are both improved.

Description

technical field [0001] The invention relates to the technical field of molten refractory profiles, in particular to a preparation method of a magnesium-erbium-cerium molten refractory profile. Background technique [0002] Refractory materials are most afraid of moisture and water immersion, and are greatly affected by the environment. In actual production and application, environmental factors are not easy to control. Products of traditional technology need to be dried at high temperature before they leave the factory for use. The steps are complicated and greatly increase cost and inconvenience to users. The above problems are technical difficulties that cannot be overcome at home and abroad for many years. [0003] Traditional process: need to go through the ratio of raw material large crystal, magnesium aluminum zirconium crystalline stone, magnesium aluminum crystalline stone - adding binder mixture - pouring into mold - extrusion molding by press - heating and drying ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/05
CPCC04B35/05C04B2235/3224C04B2235/3229C04B2235/3244C04B2235/77C04B2235/96C04B2235/9607C04B2235/9669
Inventor 任有科
Owner 任有科
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