Method for improving purity of alpaka material
A nickel-nickel-white copper, purity technology, applied in the field of material purification, can solve problems such as damage to x-ray tubes, danger, and failure to meet preparation requirements, and achieve the effect of improving purity and improving purification efficiency
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Embodiment 1
[0025] A method for improving the purity of nickel-nickel-nickel-copper material mainly comprises the following steps:
[0026] S1: Preprocessing
[0027] Pickling: Completely immerse the nickel-nickel-nickel-copper raw material in absolute ethanol, use an ultrasonic cleaning device to pickle for 10-20 minutes, and clean and dry the nickel-nickel-nickel copper raw material;
[0028] Surface treatment: put the nickel-nickel-nickel-copper raw material after pickling in the electrolyte, and pass the current density at 3-5A / cm 2 Electrolyze the surface layer of nickel-white copper with high current to remove the oxide layer on the surface of nickel-white copper, and clean the surface of nickel-white copper with a high-power blower. The electrolyte consists of 3% hydrochloric acid, 2% oxalic acid, 5% citric acid, 2% ammonium sulfate, deionized water remainder composition;
[0029] S2: vacuum induction melting
[0030] Put the pretreated nickel-nickel-nickel copper raw material i...
Embodiment 2
[0034] It is basically the same as Example 1, except that the nickel-nickel-copper raw material in S1 is subjected to a slagging and impurity removal process before pickling: the nickel-nickel-nickel raw material is heated to 1200K to obtain a melt raw material, and a mixed slagging agent is added thereto, The mass ratio of the mixed slagging agent to the melt raw material is 1:8, and the mixed slagging agent is a cone-shaped material pressed into a slagging agent, a cosolvent and a protective agent at a mass ratio of 10:9:2, and the slagging agent For CaO and SiO 2 Composed at a mass ratio of 1:1, the co-solvent is CaCl 2 , the protective agent is composed of borax and magnesium 3:1, the mixed slagging agent reacts with the impurities in the melt raw material to generate oxide residue, and the oxide residue floating on the surface of the molten raw material is removed by using the slagging equipment until There is no obvious oxide residue on the surface of the melt, and the ...
Embodiment 3
[0036] It is basically the same as Example 1, except that the nickel-nickel-copper raw material in S1 is subjected to a powder-making and impurity-removing process before pickling: the nickel-nickel-nickel raw material is cut into rod-shaped materials, and the rod-shaped materials are clamped on the smelting machine, Electrode induction melting until the rod-shaped material is melted into a liquid, the liquid falls through the settling tube under the action of gravity, and the liquid material is blown into fine droplets by using a high-temperature injection gas. The high-temperature injection gas is 600K argon, and the high-temperature injection gas The spray speed is 400m / s, and the liquid droplets condense into solid powder during the sedimentation process. The solid powder is sorted to obtain nickel-nickel-nickel powder, and the nickel-nickel-nickel powder is subjected to cold isostatic pressing to obtain the nickel-nickel-nickel raw material after impurity removal. Cold isos...
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